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公开(公告)号：US5675010A
公开(公告)日：1997-10-07
申请号：US646671
申请日：1996-05-08
IPC分类号： C07D213/20 , C07D213/61
CPC分类号： C07D213/61
摘要： The present invention relates to new chloropyridinium chlorides of the general formula (I) ##STR1## in which R.sup.1 represents in each case optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, arylalkyl or heteroarylalkyl, R.sup.2 represents optionally substituted alkyl, and R.sup.3 represents hydrogen, halogen or optionally substituted alkyl, to a process for their preparation and to their use for the preparation of chloropyridines.
摘要翻译： 本发明涉及通式（I）的新的氯代吡啶鎓氯化物，其中R 1在每种情况下均为任选取代的烷基，烯基，炔基，环烷基，环烷基烷基，芳基烷基或杂芳基烷基，R 2表示任选取代的烷基， 并且R 3表示氢，卤素或任选取代的烷基，其制备方法及其用于制备氯吡啶的用途。
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公开(公告)号：US5541332A
公开(公告)日：1996-07-30
申请号：US368179
申请日：1995-01-04
IPC分类号： C07D213/20 , C07D213/61
CPC分类号： C07D213/61
摘要： A process for the preparation of a chloropyridine of the formula ##STR1## which comprises reacting an enamide of the formula ##STR2## with a chlorinating agent in the presence of a di-substituted formamide ##STR3## in which R.sup.4 and R.sup.5 each individually is alkyl or cycloalkyl or together are alkanediyl, at a temperature between about -30.degree. C. and 100.degree. C., thereby to produce a compound of the formula ##STR4## and subjecting said compound to thermal cleavage. Compounds I are novel. Compounds IV are known intermediates for agrochemicals and pharmaceuticals.
摘要翻译： （IV）的氯吡啶的制备方法，其包括在二取代的甲酰胺（III）的存在下使式（I）的酰胺与氯化剂反应， 其中R 4和R 5各自独立地是烷基或环烷基或一起是烷二基，在约-30℃至100℃的温度下，从而产生下式化合物（I），并使所述化合物 热裂解。 化合物I是新的。 化合物IV是农药和药物的已知中间体。
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公开(公告)号：US5874586A
公开(公告)日：1999-02-23
申请号：US18484
申请日：1998-02-04
申请人： Reinhard Lantzsch , Uwe Stelzer , Carl Casser
发明人： Reinhard Lantzsch , Uwe Stelzer , Carl Casser
IPC分类号： C07D257/04 , C07D401/06 , C07D403/06
CPC分类号： C07D257/04
摘要： Herbicidally active 1-aryl-4-carbamoyl-tetrazolinones of the formula (I) ##STR1## in which Ar represents optionally substituted aryl,R.sup.1 represents in each case optionally substituted alkyl, alkenyl, alkinyl or alkoxy, andR.sup.2 represents in each case optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, aryl or arylalkyl, or, together with R.sup.1, represents alkanediyl,are obtained in good yields and at high purity by reacting 1-aryl-tetrazolinones of the formula (II) with phosgene in the presence of a diluent at temperatures of between 0.degree. C. and 150.degree. C. ("first process step"), and reacting the resulting (novel) 1-aryl-4-chlorocarbonyl-tetrazolinones of the formula (III) with amines of the formula (IV) in the presence of a diluent, and, where appropriate, in the presence of a further basic compound, at temperatures of between -20.degree. C. and +100.degree. C. ("second process step"): ##STR2##
摘要翻译： 式（I）的除草活性1-芳基-4-氨基甲酰基 - 四唑啉酮其中Ar表示任选取代的芳基，R 1表示在任何情况下为任选取代的烷基，烯基，炔基或烷氧基，并且R 2表示 通过使式（II）的1-芳基 - 四唑啉酮与式（II）的1-芳基 - 四唑啉酮反应，可以以良好的收率和高纯度获得任意取代的烷基，烯基，炔基，环烷基，环烷基烷基，芳基或芳基烷基，或者与R1一起代表烷二基， 在0℃至150℃的温度下，在稀释剂存在下进行光气（“第一工艺步骤”），并使所得式（III）的（新）1-芳基-4-氯羰基 - 四唑啉酮与式 （Ⅳ）的胺在稀释剂存在下，在适当的情况下，在另外的碱性化合物的存在下，在-20℃至+ 100℃的温度下进行。（“第二工艺步骤” ）：
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公开(公告)号：US5877323A
公开(公告)日：1999-03-02
申请号：US023060
申请日：1998-02-12
申请人： Reinhard Lantzsch , Uwe Stelzer , Carl Casser
发明人： Reinhard Lantzsch , Uwe Stelzer , Carl Casser
IPC分类号： A01N43/713 , C07D257/04
CPC分类号： C07D257/04
摘要： Herbicidally active 1-aryl-4-carbamoyl-tetrazolinones of the formula (I) ##STR1## in which Ar represents optionally substituted aryl,R.sup.1 represents in each case optionally substituted alkyl, alkenyl, alkinyl or alkoxy, andR.sup.2 represents in each case optionally substituted alkyl, alkenyl, alkinyl, cycloalkyl, cycloalkylalkyl, aryl or arylalkyl, or, together with R.sup.1, represents alkanediyl,are obtained in good yields and at high purity by reacting 1-aryl-tetrazolinones of the formula (II) with phosgene in the presence of a diluent at temperatures of between 0.degree. C. and 150.degree. C. ("first process step"), and reacting the resulting (novel) 1-aryl-4-chlorocarbonyl-tetrazolinones of the formula (III) with amines of the formula (IV) in the presence of a diluent, and, where appropriate, in the presence of a further basic compound, at temperatures of between -20.degree. C. and +100.degree. C. ("second process step"): ##STR2##
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公开(公告)号：US6166256A
公开(公告)日：2000-12-26
申请号：US566073
申请日：2000-05-08
申请人： Henry Giera , Carl Casser , Pieter Ooms , Michael Schelhaas , Christian Laue , Michaela Meiers , Gerhard Braun
发明人： Henry Giera , Carl Casser , Pieter Ooms , Michael Schelhaas , Christian Laue , Michaela Meiers , Gerhard Braun
IPC分类号： B01J31/02 , C07B61/00 , C07C239/10 , C07C239/00
CPC分类号： C07C239/10
摘要： The present invention provides a process for preparing (4-nitroso-phenyl)phenyl-hydroxylamine which is characterized in that nitrobenzene is reacted in the presence of hydroxide and/or oxide-containing bases, optionally in the presence of solvents, at temperatures of 20 to 180.degree. C. and pressures of 0.1 to 10 bar.The process according to the invention has the particular advantage that it uses inexpensive and cost-effective nitrobenzene as starting material instead of the nitrosobenzene conventionally used hitherto.
摘要翻译： 本发明提供一种制备（4-亚硝基苯基）苯基羟胺的方法，其特征在于硝酸苯在含氢氧化物和/或氧化物的碱存在下，任选地在溶剂存在下，在20℃的温度下反应 至180℃，压力为0.1至10巴。 根据本发明的方法具有特别的优点，它使用廉价且具有成本效益的硝基苯作为起始原料，而不是迄今为止常规使用的亚硝基苯。
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公开(公告)号：US6054589A
公开(公告)日：2000-04-25
申请号：US118954
申请日：1998-07-17
IPC分类号： B01J27/06 , B01J27/14 , C07B61/00 , C07D491/04 , C07D491/056 , C07D235/02
CPC分类号： C07D491/04
摘要： A novel process for the preparation of 2-chloro-benzimidazole derivatives of the formula ##STR1## in which A represents optionally halogenated alkylene having 1 or 2 carbon atoms,which process comprises reaction 1,3-dihydro-benzimidazol(ethi)ones of the formula ##STR2## in which X represents oxygen or sulphur,with phosphorus oxychloride.Novel 1,3-dihydro-benzimidazol(ethi)ones of the formula(II) and process for their preparation.
摘要翻译： 一种用于制备下式的2-氯 - 苯并咪唑衍生物的新方法，其中A表示任选地具有1或2个碳原子的卤代亚烷基，该方法包括下式的反应1,3-二氢 - 苯并咪唑（ethi），其中 X表示氧或硫，与磷酰氯反应。 新的式（II）的1,3-二氢 - 苯并咪唑（ethi）及其制备方法。
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公开(公告)号：US5814669A
公开(公告)日：1998-09-29
申请号：US765470
申请日：1996-12-20
申请人： Uwe Stelzer , Carl Casser , Thomas Seitz
发明人： Uwe Stelzer , Carl Casser , Thomas Seitz
IPC分类号： C07D263/44 , A01N37/18 , A01N37/20 , A01N37/44 , A01N43/16 , C07C231/02 , C07C237/02 , C07C237/06 , C07C237/08 , C07C269/04 , C07C271/04 , C07C271/06 , C07C271/22 , C07D311/58 , A61K31/165 , C07C231/10 , C07C233/05
CPC分类号： A01N43/16 , A01N37/44 , C07C237/02 , C07C237/06 , C07C237/08 , C07C269/04 , C07D311/58
摘要： The invention relates to novel amino acid derivatives, to a process for their preparation and to their use as pesticides, in particular as fungicides, and as intermediates for preparing known substituted amino acid derivatives with fungicidal activity.
摘要翻译： PCT No.PCT / EP95 / 02321 Sec。 371日期1996年12月20日第 102（e）日期1996年12月20日PCT提交1995年6月16日PCT公布。 出版物WO96 / 00718 日期1996年1月1日本发明涉及新型氨基酸衍生物，其制备方法及其作为农药，特别是作为杀真菌剂的用途，以及用于制备具有杀真菌活性的已知取代的氨基酸衍生物的中间体。
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公开(公告)号：US5621119A
公开(公告)日：1997-04-15
申请号：US502340
申请日：1995-07-14
IPC分类号： A61K6/083 , C07D317/36 , A61C13/23
CPC分类号： C07D317/36 , A61K6/083
摘要： The invention relates to diacrylates and dimethacrylates having cyclic carbonate groups, and their use in dental materials.
摘要翻译： 本发明涉及具有环状碳酸酯基团的二丙烯酸酯和二甲基丙烯酸酯，以及它们在牙科材料中的应用。
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公开(公告)号：US5227458A
公开(公告)日：1993-07-13
申请号：US860831
申请日：1992-03-31
申请人： Dieter Freitag , Uwe Westeppe , Claus H. Wulff , Karl-Herbert Fritsch , Carl Casser , Gunther Weymans , Lutz Schrader , Werner Waldenrath
发明人： Dieter Freitag , Uwe Westeppe , Claus H. Wulff , Karl-Herbert Fritsch , Carl Casser , Gunther Weymans , Lutz Schrader , Werner Waldenrath
CPC分类号： B01D71/50 , C07C39/17 , C08G64/06 , C07C2101/14 , Y10T428/31507
摘要： Dihydroxydiphenyl cycloalkanes corresponding to the formula ##STR1## in which R.sup.1 and R.sup.2 independently of one another represent hydrogen, halogen, C.sub.1 -C.sub.8 alkyl, C.sub.5 -C.sub.6 cycloalkyl, C.sub.6 -C.sub.10 aryl and C.sub.7 -C.sub.12 aralkyl,m is an integer of from 4 to 7,R.sup.3 and R.sup.4, individually selectable for each X, independently of one another represent hydrogen or C.sub.1 -C.sub.6 alkylandX represents carbon with the proviso that, at at least one atom X, both R.sup.3 and R.sup.4 are alkyl,a process for their production, their use for the production of high molecular weight polycarbonates, the polycarbonates made from dihydroxydiphenyl cycloalkane of formula (I) and films made from these polycarbonates.
摘要翻译： 对应于式（I）的二羟基二苯基环烷烃，其中R 1和R 2彼此独立地表示氢，卤素，C 1 -C 8烷基，C 5 -C 6环烷基，C 6 -C 10芳基和C 7 -C 12芳烷基，m是整数 4至7个，每个X独立地各自独立地选择R 3和R 4表示氢或C 1 -C 6烷基，X表示碳，条件是在至少一个原子X，R 3和R 4均为烷基时， 其制备方法，其用于生产高分子量聚碳酸酯，由式（I）的二羟基二苯基环烷烃制成的聚碳酸酯和由这些聚碳酸酯制成的薄膜。
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公开(公告)号：US5210328A
公开(公告)日：1993-05-11
申请号：US904186
申请日：1992-06-25
申请人： Dieter Freitag , Claus H. Wulff , Alfred Eitel , Helmut Waldmann , Uwe Westeppe , Manfred Hajek , Klaus D. Berg , Bernd Griehsel , Carl Casser
发明人： Dieter Freitag , Claus H. Wulff , Alfred Eitel , Helmut Waldmann , Uwe Westeppe , Manfred Hajek , Klaus D. Berg , Bernd Griehsel , Carl Casser
CPC分类号： C07C37/20 , C07C2101/14
摘要： This invention relates to a process for the preparation of substituted cycloalkylidene bisphenols from phenols and special cycloalkanones in the presence of acid condensation catalysts and in the presence of water.
摘要翻译： 本发明涉及一种在酸性缩合催化剂存在下和在水存在下由酚和特殊的环烷酮制备取代的环亚烷基双酚的方法。
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