摘要:
There are disclosed a 4-alkoxy-1,3-dioxane-5-carbonitrile which is a novel compound represented by the formula ##STR1## wherein R represents a lower-alkyl group, and which is useful as an intermediate for the synthesis of Vitamin B.sub.1, and a process for preparing the novel compound by subjecting a 3-alkoxy-2-propenenitrile to reaction with a formaldehyde in the presence of an acid catalyst.
摘要:
There is disclosed a process for the preparation of a 2-alkyl-4-amino-5-aminomethylpyrimidine, which comprises subjecting a 2-alkyl-4-amino-5-formylpyrimidine to catalytic reaction with hydrogen and ammonia in the presence of a reduction catalyst.According to the process of this invention, the desired product can be obtained in much higher yield as compared with the processes known to the art.
摘要:
A process for preparing a 4-amino-5-dialkoxymethylpyrimidine derivative of the formula: ##STR1## which comprises reacting a propanenitrile derivative represented by the formula (I) or the novel compound represented by formula (II): ##STR2## with an amidine of the formula: ##STR3## wherein R.sup.1 to R.sup.6 are as defined in the specification. Also disclosed is a process for making the novel compounds of formula (II).
摘要:
A process for preparing an N-alkylene-diamine by contacting an alkylene diamine with an aliphatic aldehyde in a reaction solvent in the presence of hydrogen under pressure and an platinum group metal, which comprises gradually adding the aliphatic aldehyde to the alkylene diamine. The process according to the present invention provides a high conversion of the alkylene diamine and a high selectivity to the N-alkyl-alkylene-diamine.
摘要:
[Object]To provide a calculation method and calculation device for an average sublimation interface temperature, bottom part temperature, and sublimation rate of the whole to-be-dried material introduced into a drying chamber of a freeze-drying device without contaminating or collapsing the to-be-dried material.[Solution]The present invention is applied to a freeze-drying device that includes a drying chamber DC, a cold trap CT, vacuum adjustment means for adjusting the degree of the vacuum in the drying chamber DC, and a control device CR for automatically controlling the operations of the above elements. The control device CR stores a required relational expression and a calculation program, drives the vacuum adjusting means during a primary drying period of the to-be-dried material to temporarily change the drying chamber's degree of vacuum Pdc in an increasing direction, and calculates the average sublimation interface temperature Ts, bottom part temperature Tb, and sublimation rate Qm of the to-be-dried material during the primary drying period in accordance with the relational expression and with measured data including the drying chamber's degree of vacuum Pdc and the cold trap's degree of vacuum Pdt, which are obtained before and after the temporary change.
摘要:
The invention provides a control apparatus and a control method for a vehicle provided with an automatic transmission which has an automatic shift mode in which a gear is selected according to a running state and a manual shift mode in which a gear is selected according to a manual operation, and which transmits driving force generated by an internal combustion engine. The control apparatus and control method determine whether the vehicle is in a high load state; determine whether engine braking force from the internal combustion engine is required; calculate differential braking force which is the difference between engine braking force generated when running in a gear selected according to the manual operation and engine braking force generated when running in a gear selected according to the running state; and control the automatic transmission to execute an upshift and perform control to generate the calculated differential braking force when it is determined that i) the vehicle is in the high load state and ii) the engine braking force is required, while the automatic transmission is in the manual shift mode.
摘要:
The present invention provides a white smoke generating apparatus for generating white smoke of a stable density unaffected by air temperature or humidity conditions. The apparatus comprises an apparatus main body 11 being provided with a white smoke discharge opening 11a; a cryogenic liquefied gas supply mechanism 12 for supplying a cryogenic liquefied gas into the apparatus main body 11; and a humidifying mechanism 13 for humidifying the atmosphere inside the apparatus main body. The cryogenic liquefied gas supply mechanism 12 is provided with a first pipeline 18 which communicates a cryogenic liquefied gas reservoir 16 and a cryogenic liquefied gas emission nozzle 17 placed inside the apparatus main body 11, preferably at the white smoke discharge opening 11a side. The humidifying mechanism 13 comprises a second pipeline 24 which branches from the first pipeline 18 and communicates with a spray nozzle 21 placed inside the apparatus main body 11 for spraying water, and a third pipeline 28 which branches from the second pipeline 24 and communicates with the spray nozzle 21 via a water reservoir 25. A cryogenic liquefied gas vaporizer 22 is provided inside the second pipeline 24 upstream from the point where the third pipeline 28 branches from the second pipeline 24.
摘要:
The present invention relates to a mold for producing glass articles comprising a glass-made mold base, an intermediate layer formed by a silicon carbide and/or silicon nitride film, and an uppermost layer formed by a carbon film. Since the mold for producing glass articles exhibits an excellent bonding between the glass-made mold base and the uppermost layer formed by the carbon film, peeling of the uppermost layer can be prevented. Therefore, the function of the uppermost layer as an adhesion-prevention layer against the glass to be molded can be exhibited for a long time, causing an economic advantage since the life of the mold can be lengthened. In addition, since the maximum surface roughness of the working surface of the mold can be reduced and the surface shape accuracy can be maintained, a molded glass article exhibits excellent surface accuracy without optical defects.
摘要:
A program is executed which includes a step (S100) of calculating a base required driving force, a step (S200) of calculating a reference driving force, a step (S400) of calculating a final required driving force on which a vibration suppression filtering process has been performed when the base required driving force is greater than a reference driving force, and a step (S500) of calculating a final required driving force on which the vibration suppression filtering process has not been performed when the base required driving force is equal to or less than the reference driving force.
摘要:
A vehicle control device for executing the following control are provided. When a driving mode is input, a CPU of an ECU outputs an instruction for shifting a power transfer mechanism in accordance with the input driving mode, and controls a power control mechanism in accordance with a stored driving mode. When it is determined that shifting of the power transfer mechanism has been completed, the CPU switches the characteristic of the power control mechanism in accordance with the input driving mode. On the other hand, when it is determined that a predetermined period of time has elapsed without completing the shifting from when the instruction for shifting the power transfer mechanism is issued, the CPU maintains the characteristic of the power control mechanism at a characteristic corresponding to the stored driving mode.