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公开(公告)号：US20170051390A1
公开(公告)日：2017-02-23
申请号：US15059806
申请日：2016-03-03
发明人： Juchang Miao , Yong Zhai , Jianxin Ma , Enfeng Gao , Yanling Song , Shulin Diao , Yi Dong , Haibo Yi , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
IPC分类号： C23C14/04
CPC分类号： C23C14/046 , F27D3/0024 , F27D7/02 , F27D19/00 , F27D21/00 , F27D2003/0034 , H01F41/0293
摘要： An infiltration device comprises a heating room, a rotary tray, a rotary bracket, a material box, an elevating mechanism and a transmission device, wherein the heating room has an annular groove, and the rotary tray is arranged below an opening end at a lower end of the heating room; the rotary bracket is installed on the rotary tray; the material box is arranged on the rotary bracket; the rotary tray and the material box can move upward and downward under the action of the elevating mechanism; the rotary bracket can spin in the annular groove and revolve around a central axis of the rotary tray under the action of the transmission device. The infiltration method provided by the invention comprises the steps of charging, vacuum-pumping, high temperature infiltrating, cooling, discharging, etc.
摘要翻译： 渗透装置包括加热室，旋转托盘，旋转托架，材料箱，升降机构和传动装置，其中加热室具有环形槽，并且旋转托盘布置在较低的开口端的下方 加热室结束; 旋转支架安装在转盘上; 材料盒布置在旋转支架上; 旋转托盘和料箱可在升降机构的作用下向上和向下移动; 旋转支架可以在传动装置的作用下旋转在环形槽中并围绕转盘的中心轴线旋转。 本发明提供的渗透方法包括充电，真空抽吸，高温渗透，冷却，放电等步骤。
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公开(公告)号：US10269488B2
公开(公告)日：2019-04-23
申请号：US15060188
申请日：2016-03-03
发明人： Haibo Yi , Yi Dong , Shulin Diao , Yi Yuan , Shujie Wu , Cailing Sun , Juchang Miao , Ya Chen , Wenjie Yuan
摘要： The present invention provides a method for preparing a permanent magnet material, the method comprising coating step and infiltrating step, wherein, coating a rare earth element-containing substance on the surface of a permanent magnet, the magnet having a thickness of 10 mm or less at least in one direction, then placing the magnet into a container, vacuuming to an atmospheric pressure of below 10 Pa, closing the passageway, and then heat treating the closed container. Using the method of the present invention enables the rare earth element to infiltrate homogeneously with a high permeability. In addition, the present invention may have a lower production cost, significantly increase coercive force of the permanent magnet material, but decrease the remanence very little.
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公开(公告)号：US10109401B2
公开(公告)日：2018-10-23
申请号：US15060267
申请日：2016-03-03
发明人： Shujie Wu , Yi Dong , Shulin Diao , Haibo Yi , Yichuan Wang , Zhanjiang Hu , Juchang Miao , Yi Yuan , Ya Chen , Wenjie Yuan
摘要： The present invention provides a method for improving coercive force of magnets, this method comprises steps as follows: S2) coating step: coating a coating material on the surface of a magnet and drying it; and S3) infiltrating step: heat treating the magnet obtained from the coating step S2). The coating material comprises (1) metal calcium particles and (2) particles of a material containing a rare earth element; the rare earth element is at least one selected from Praseodymium, Neodymium, Gadolinium, Terbium, Dysprosium, Holmium, Erbium, Thulium, Ytterbium and Lutetium. The method of the present invention can significantly increase coercive force of a permanent magnet material, while remanence and magnetic energy product hardly decrease. In addition, the method of the present invention can significantly decrease the amount of a rare earth element, and accordingly, decrease the production cost.
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公开(公告)号：US10381140B2
公开(公告)日：2019-08-13
申请号：US15060104
申请日：2016-03-03
发明人： Shulin Diao , Yi Dong , Haibo Yi , Yuelin Fan , Juchang Miao , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
摘要： The present invention provides a method for preparing a rare earth permanent magnet material. The preparation method of the present invention comprises atomizing spray process and infiltrating process, wherein the atomizing-sprayed sintered rare earth magnet is placed in a closed container before infiltrating. Through the atomizing spray process a solution containing a heavy rare earth element is coated on the surface of a sintered R1-Fe(Co)—B-A-X-M rare earth magnet, and after baking, heat treatment is performed to infiltrate the sprayed heavy rare earth element to the grain boundary phase of the sintered rare earth magnet. This method decreases the amount of a heavy rare earth element used, increases the coercive force of magnets with a little decrease of remanence, decreases the remanence temperature coefficient and coercive force temperature coefficient of the magnet, and improves resistance of the magnet against demagnetization at a high temperature.
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公开(公告)号：US09889474B2
公开(公告)日：2018-02-13
申请号：US15059736
申请日：2016-03-03
发明人： Juchang Miao , Yong Zhai , Jianxin Ma , Enfeng Gao , Yanling Song , Shulin Diao , Yi Dong , Haibo Yi , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
IPC分类号： B05B13/02 , B05B15/04 , B05B7/06 , B08B3/00 , B05B7/08 , B05B3/00 , B05B13/04 , H01F1/057 , B05B15/00 , B05D1/02 , B05D3/02 , B05B15/02 , B65G45/22
CPC分类号： B08B3/00 , B05B3/00 , B05B7/0807 , B05B13/0221 , B05B13/0478 , B05B14/20 , B05B14/30 , B05B15/00 , B05B15/25 , B05B15/50 , B05B15/52 , B05B15/55 , B05B16/40 , B05D1/02 , B05D3/0218 , B05D2252/10 , B05D2258/02 , B65G45/22 , H01F1/0575 , Y02P70/36
摘要： A spraying device comprises: a conveyer comprising a mesh crawler belt configured to carry an object to be sprayed; a baking chamber for heating the object to be sprayed; a spraying chamber having at least one atomizing nozzle disposed within the spraying chamber, the atomizing nozzle being configured to uniformly spray a coating solution on a surface of the object to be sprayed; a cleaning chamber for cleaning the mesh crawler belt and recycling the coating solution carried by the mesh crawler belt; and a solution storage apparatus for storing the coating solution that the spraying chamber needs for spraying; wherein the mesh crawler belt passes successively through the baking chamber, the spraying chamber and the cleaning chamber. The device of the present invention can ensure uniformity of the thickness of a coating layer on the magnet. In addition, the device can improve spraying efficiency and save raw material.
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公开(公告)号：US20170062104A1
公开(公告)日：2017-03-02
申请号：US15060104
申请日：2016-03-03
发明人： Shulin Diao , Yi Dong , Haibo Yi , Yuelin Fan , Juchang Miao , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
CPC分类号： H01F1/055 , B22F3/24 , B22F9/023 , B22F9/04 , B22F2003/248 , B22F2009/044 , H01F1/0536 , H01F1/0577 , H01F41/0293
摘要： The present invention provides a method for preparing a rare earth permanent magnet material. The preparation method of the present invention comprises atomizing spray process and infiltrating process, wherein the atomizing-sprayed sintered rare earth magnet is placed in a closed container before infiltrating. Through the atomizing spray process a solution containing a heavy rare earth element is coated on the surface of a sintered R1-Fe(Co)—B-A-X-M rare earth magnet, and after baking, heat treatment is performed to infiltrate the sprayed heavy rare earth element to the grain boundary phase of the sintered rare earth magnet. This method decreases the amount of a heavy rare earth element used, increases the coercive force of magnets with a little decrease of remanence, decreases the remanence temperature coefficient and coercive force temperature coefficient of the magnet, and improves resistance of the magnet against demagnetization at a high temperature.
摘要翻译： 本发明提供稀土永磁材料的制备方法。 本发明的制备方法包括雾化喷雾工艺和渗透方法，其中雾化喷射烧结稀土磁体在渗透之前置于密闭容器中。 通过雾化喷雾法，将含有重稀土元素的溶液涂覆在烧结的R1-Fe（Co）-BAXM稀土磁体的表面上，烘烤后进行热处理，将喷射后的重稀土元素 烧结稀土磁体的晶界相。 该方法减少了所使用的重稀土元素的量，增加了磁铁的矫顽力，同时减少了磁铁的剩磁温度系数和矫顽力温度系数，从而提高了磁体的抗磁化能力。 高温。
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公开(公告)号：US20170050222A1
公开(公告)日：2017-02-23
申请号：US15059736
申请日：2016-03-03
发明人： Juchang Miao , Yong Zhai , Jianxin Ma , Enfeng Gao , Yanling Song , Shulin Diao , Yi Dong , Haibo Yi , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
CPC分类号： B08B3/00 , B05B3/00 , B05B7/0807 , B05B13/0221 , B05B13/0478 , B05B14/20 , B05B14/30 , B05B15/00 , B05B15/25 , B05B15/50 , B05B15/52 , B05B15/55 , B05B16/40 , B05D1/02 , B05D3/0218 , B05D2252/10 , B05D2258/02 , B65G45/22 , H01F1/0575 , Y02P70/36
摘要： A spraying device comprises: a conveyer comprising a mesh crawler belt configured to carry an object to be sprayed; a baking chamber for heating the object to be sprayed; a spraying chamber having at least one atomizing nozzle disposed within the spraying chamber, the atomizing nozzle being configured to uniformly spray a coating solution on a surface of the object to be sprayed; a cleaning chamber for cleaning the mesh crawler belt and recycling the coating solution carried by the mesh crawler belt; and a solution storage apparatus for storing the coating solution that the spraying chamber needs for spraying; wherein the mesh crawler belt passes successively through the baking chamber, the spraying chamber and the cleaning chamber. The device of the present invention can ensure uniformity of the thickness of a coating layer on the magnet. In addition, the device can improve spraying efficiency and save raw material.
摘要翻译： 喷涂装置包括：输送机，包括构造成承载待喷涂物体的网状履带; 用于加热被喷射物体的烘烤室; 喷雾室，其具有设置在所述喷雾室内的至少一个雾化喷嘴，所述雾化喷嘴构造成在被喷射物体的表面上均匀地喷射涂布液; 用于清洁网状履带并将由网状履带带出的涂布液再循环的清洗室; 以及用于储存喷雾室需要喷涂的涂布溶液的溶液存储装置; 其中网状履带通过烘烤室，喷雾室和清洁室。 本发明的装置可以确保磁体上涂层的厚度均匀。 此外，该设备可以提高喷涂效率并节省原材料。
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公开(公告)号：US10138540B2
公开(公告)日：2018-11-27
申请号：US15059806
申请日：2016-03-03
发明人： Juchang Miao , Yong Zhai , Jianxin Ma , Enfeng Gao , Yanling Song , Shulin Diao , Yi Dong , Haibo Yi , Shujie Wu , Yi Yuan , Ya Chen , Wenjie Yuan
摘要： An infiltration device comprises a heating room, a rotary tray, a rotary bracket, a material box, an elevating mechanism and a transmission device, wherein the heating room has an annular groove, and the rotary tray is arranged below an opening end at a lower end of the heating room; the rotary bracket is installed on the rotary tray; the material box is arranged on the rotary bracket; the rotary tray and the material box can move upward and downward under the action of the elevating mechanism; the rotary bracket can spin in the annular groove and revolve around a central axis of the rotary tray under the action of the transmission device. The infiltration method provided by the invention comprises the steps of charging, vacuum-pumping, high temperature infiltrating, cooling, discharging, etc.
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公开(公告)号：US20180226189A1
公开(公告)日：2018-08-09
申请号：US15842039
申请日：2017-12-14
发明人： Shujie Wu , Yi Dong , Shulin Diao , Shuai Zhang , Yi Yuan , Ya Chen , Wenjie Yuan
CPC分类号： H01F41/0266 , C25D3/665 , C25D5/18 , C25D5/50 , C25D7/001 , H01F1/0536 , H01F1/0577 , H01F41/0293
摘要： The disclosure discloses a method for preparing a permanent magnet material. In this method, an ionic liquid electroplating process is used to electroplate a heavy rare earth metal onto a surface of a sintered magnet to form a magnet with a coating, wherein the sintered magnet has a thickness of 10 mm or less in at least one direction; in the ionic liquid electroplating process, an electroplating solution comprises an ionic liquid, a heavy rare earth salt, a group VIII metal salt, an alkali metal salt and an additive, an anode is a heavy rare earth metal or a heavy rare earth alloy, a cathode is the sintered magnet, an electroplating temperature is 20-50° C., an electroplating time is 15-80 min. The preparation method of the disclosure can improve an intrinsic coercive force of the magnet with low cost and high production efficiency. A utilization rate of heavy rare earth is high.
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公开(公告)号：US20170062127A1
公开(公告)日：2017-03-02
申请号：US15060188
申请日：2016-03-03
发明人： Haibo Yi , Yi Dong , Shulin Diao , Yi Yuan , Shujie Wu , Cailing Sun , Juchang Miao , Ya Chen , Wenjie Yuan
CPC分类号： H01F41/0266 , B22F3/12 , B22F3/24 , B22F3/26 , B22F2003/248 , C21D6/00 , H01F1/0577 , H01F41/005 , H01F41/0293
摘要： The present invention provides a method for preparing a permanent magnet material, the method comprising coating step and infiltrating step, wherein, coating a rare earth element-containing substance on the surface of a permanent magnet, the magnet having a thickness of 10 mm or less at least in one direction, then placing the magnet into a container, vacuuming to an atmospheric pressure of below 10 Pa, closing the passageway, and then heat treating the closed container. Using the method of the present invention enables the rare earth element to infiltrate homogeneously with a high permeability. In addition, the present invention may have a lower production cost, significantly increase coercive force of the permanent magnet material, but decrease the remanence very little.
摘要翻译： 本发明提供一种永久磁铁材料的制备方法，其特征在于，包括上述步骤和渗透工序，其中，在永久磁铁表面上涂覆含有稀土元素的物质，其厚度为10mm以下 至少在一个方向上，然后将磁体放置在容器中，抽真空至低于10Pa的大气压力，关闭通道，然后热处理密闭容器。 使用本发明的方法能够使稀土元素以高渗透性均匀地渗透。 此外，本发明可以具有较低的生产成本，显着增加了永久磁铁材料的矫顽力，但是减少了剩磁。
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