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公开(公告)号:US12123102B1
公开(公告)日:2024-10-22
申请号:US18424203
申请日:2024-01-26
CPC分类号: C25D13/18 , C01G3/02 , C25D13/02 , C01P2004/03
摘要: A method of forming a highly textured tenorite film includes providing a substrate in a pulsed electrophoretic deposition (PEPD) reactor. Tenorite microcrystals, de-ionized water, hydrogen peroxide and sulfuric acid are mixed in the PEPD reactor. A temperature of the PEPD reactor is adjusted to 2-15° C. The highly textured tenorite film is formed on the substrate by electrophoresis having electrophoretic parameters. The electrophoretic parameters include a pulse ON time having a duration of 10 ms to 500 ms, a pulse duty cycle having a range of 0.1 to 0.23, a pulse height having a range of 0.1 to 0.8 kilovolts, and a deposition time having a range of 70 minutes to 2.5 hours.
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公开(公告)号:US12090169B2
公开(公告)日:2024-09-17
申请号:US18599582
申请日:2024-03-08
发明人: Muhammad Nawaz , Firdos Alam Khan
CPC分类号: A61K33/38 , A61K9/14 , A61P35/00 , C01B25/45 , C01G3/02 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2002/85 , C01P2004/03 , C01P2004/32 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要: A method of making Cu—Ag3PO4 nanoparticles is provided. The method includes forming a mixture of at least one silver salt, at least one phosphate salt, and at least one copper (II) salt. The method further includes dissolving the mixture in water. The method further includes sonicating the mixture. The method further includes precipitating the Cu—Ag3PO4 nanoparticles or “nanoparticles”. The copper is present in the nanoparticles in an amount of 2 to 23 weight percent (wt. %) based on the total weight of the Cu—Ag3PO4. The nanoparticles of the present disclosure find application in treating cervical cancer, and colorectal cancer. The nanoparticles may also be used in photodegrading environmental pollutants.
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公开(公告)号:US20240199438A1
公开(公告)日:2024-06-20
申请号:US18504209
申请日:2023-11-08
发明人: TAKESHI KOIWASAKI , TAKESHI UEDA , HISAO NAGAI , TAKAFUMI OKUMA
IPC分类号: C01G3/02 , B01J21/06 , B01J23/72 , B01J35/39 , B01J37/34 , C01G23/047 , C09D133/06 , C08K3/22
CPC分类号: C01G3/02 , B01J21/063 , B01J23/72 , B01J35/39 , B01J37/34 , C01G23/047 , C09D133/06 , C01P2004/62 , C01P2004/64 , C08K2003/2241 , C08K2003/2248
摘要: A composite microparticle manufacturing method includes: a step of preparing a first selective element-containing raw material and a second selective element-containing raw material, the first selective element-containing raw material containing one or more first selective elements selected from a copper element, a molybdenum element, and a silver element, the second selective element-containing raw material containing one or more second selective elements selected from titanium, germanium, silicon, tin, aluminum, zinc, zirconium, hafnium, iron, yttrium, niobium, tantalum, calcium, magnesium, indium, tungsten, molybdenum, and nickel; and a composite microparticle generation step of introducing both of the prepared raw materials into thermal plasma, evaporating the raw materials, and cooling the evaporated raw materials to generate composite microparticles including base particles and first selective element-containing microparticles being present on surfaces of the base particles, the base particles having an average particle diameter of from 10 nm to 300 nm inclusive.
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公开(公告)号:US20230355667A1
公开(公告)日:2023-11-09
申请号:US18343812
申请日:2023-06-29
发明人: Muhammad NAWAZ , Firdos Alam KHAN
CPC分类号: A61K33/38 , A61K9/14 , A61P35/00 , C01B25/45 , C01G3/02 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2002/85 , C01P2004/03 , C01P2004/32 , C01P2006/12 , C01P2006/14 , C01P2006/16
摘要: A method of making Cu-Ag3PO4 nanoparticles is provided. The method includes forming a mixture of at least one silver salt, at least one phosphate salt, and at least one copper (II) salt. The method further includes dissolving the mixture in water. The method further includes sonicating the mixture. The method further includes precipitating the Cu-Ag3PO4 nanoparticles or “nanoparticles”. The copper is present in the nanoparticles in an amount of 2 to 23 weight percent (wt.%) based on the total weight of the Cu-Ag3PO4. The nanoparticles of the present disclosure find application in treating cervical cancer, and colorectal cancer. The nanoparticles may also be used in photodegrading environmental pollutants.
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公开(公告)号:US11718537B2
公开(公告)日:2023-08-08
申请号:US17210178
申请日:2021-03-23
申请人: KING SAUD UNIVERSITY
发明人: Ali Aldalbahi , Raneem Aldawish , Manal Ahmed Gasmelseed Awad , Noura Saleem Aldosari , Reem Hamad Alshathri , Leen Abdullah Aldwihi , Raghad Alammari , Khloud Ibrahim Bin Shoqiran
IPC分类号: C01G3/02 , A01N59/20 , B01J35/00 , B01J35/02 , B01J23/72 , C08G69/48 , B82Y30/00 , B82Y40/00
CPC分类号: C01G3/02 , A01N59/20 , B01J23/72 , B01J35/004 , B01J35/023 , C08G69/48 , B82Y30/00 , B82Y40/00 , C01P2004/64
摘要: A method of synthesizing copper oxide nanoparticles includes preparing a liquid extract of Rumex vesicarius, dissolving copper salt in the liquid extract to provide a solution with copper nanoparticles, adding a base to the solution with copper nanoparticles to form a precipitate including copper oxide nanoparticles. Copper oxide nanoparticles prepared according to the method are effective photocatalysts for degrading organic dyes and antibacterial agents and exhibit anticancer activities.
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公开(公告)号:US20230027568A1
公开(公告)日:2023-01-26
申请号:US17782535
申请日:2020-12-04
摘要: A method of producing copper oxide powder includes a high-purity copper acidic solution preparation step (S01) of preparing an acidic solution containing 99.99% by mass or more of copper regarding metal components as 100% by mass, an organic acid salt addition step (S02) of adding an organic acid salt to this high-purity copper acidic solution, an organic acid copper production step (S03) of generating an organic acid copper by reacting the added organic acid salt with copper ions, an organic acid copper recovery step (S04) of recovering the obtained organic acid copper, and a heating step (S05) of forming copper oxide powder by heating the recovered organic acid copper, in which the organic acid forming the organic acid salt has 10 or less carbon atoms, and copper oxide powder.
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公开(公告)号:US20220396495A1
公开(公告)日:2022-12-15
申请号:US17835338
申请日:2022-06-08
摘要: A copper oxide crystallite having an average particle size that is greater than or equal to 5 nm and less than or equal to 15 nm, a ratio of (−111)/(111) greater than or equal to 0.5 and less than or equal to 1.5, and a blackness My greater than or equal to 130 and less than or equal to 170. The copper oxide crystallite has a reflectivity in the visible spectrum of electromagnetic radiation that is less than or equal to 10.0%, and a reflectivity in the near-IR and LiDAR spectrum of electromagnetic radiation that is greater than or equal to 10%.
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公开(公告)号:US11001505B1
公开(公告)日:2021-05-11
申请号:US16903183
申请日:2020-06-16
申请人: KING SAUD UNIVERSITY
发明人: Ali Aldalbahi , Bushra Ibarahim Alabdullah , Manal Ahmed Gasmelseed Awad , Shaykha Mohammed Alzahly , Zainah Ali Alqahtani , Shorouq Mohsen Alsaggaf , Hessa Abdullah Aljasser , Hind Ali Abdullah Alshehri
摘要: The copper oxide nanoparticles synthesized using Rhatany root extract involves preparing the Rhatany root extract by adding powdered Rhatany roots to boiling water, allowing the mixture to soak overnight, and removing any solid residue by filtering to obtain the aqueous extract. The copper oxide nanoparticles are prepared by mixing equal volumes of the aqueous Rhatany root extract and 0.1 M aqueous copper sulfate, heating the mixture at 80° C. for 40 minutes, and adding 1 M sodium hydroxide dropwise to the mixture to precipitate CuO. The precipitate is removed by centrifuge, washed with ethanol, dried, and calcined at 400° C. for 4 hours to obtain the copper oxide nanoparticles. The resulting nanoparticles proved effective in degrading wastewater dyes, showed anticancer activity against human cervical cancer by cell viability assay, and showed antibacterial activity against various strains of bacteria by agar diffusion.
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公开(公告)号:US10998467B2
公开(公告)日:2021-05-04
申请号:US16892493
申请日:2020-06-04
发明人: Ariel Antonio Franco , Ronen Sarusi
IPC分类号: H01L33/28 , C01G3/00 , A61L15/32 , A61L15/44 , C01G9/02 , H01L33/00 , H01L33/06 , H01L33/44 , C01G3/02 , B82Y20/00 , B82Y30/00 , B82Y40/00
摘要: The present invention provides composition comprising a metal oxide semiconductor nanomaterial coated or dispersed with a hemostatic polymer.
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公开(公告)号:US10981799B2
公开(公告)日:2021-04-20
申请号:US16390788
申请日:2019-04-22
申请人: FUJIFILM Corporation
发明人: Kazunori Takahashi
摘要: A fine particle in which a surface of a copper oxide fine particle (a) is coated with a coating layer (b) containing a monovalent copper compound, in which the fine particle has a specific surface area of 100 m2/g or greater, an average primary particle diameter in a range of 5 to 20 nm, and an average secondary particle diameter in a range of 5 to 50 nm, is provided.
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