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    Synthesis of triarylsulfonium salts
    3.
    发明授权
    Synthesis of triarylsulfonium salts 失效
    三芳基锍盐的合成

    公开(公告)号：US4980492A

    公开(公告)日：1990-12-25

    申请号：US317235

    申请日：1989-02-28

    Applicant: John L. Dektar ,  Nigel P. Hacker

    Inventor： John L. Dektar ,  Nigel P. Hacker

    IPC: C07F9/06 ,  C07F9/68 ,  C07F9/92

    CPC classification number: C07C381/12

    Abstract: A triarylsulfonium salt is prepared in high yield and high purity by a two-step process involving a aryl Grignard reagent reacted with a diarylsulfoxide in a solvent which is a mixture of aliphatic and aromatic hydrocarbons, followed by a second step which is metathesis with ZMF.sub.6, where Z is a metal or metal-like anion, and M is antimony, arsenic or phosphorus, preferably employing an ammonium salt and carried out in a non-aqueous solvent.

    Abstract translation: 通过两步法制备三芳基锍盐，该方法涉及在与脂族和芳族烃的混合物的溶剂中与二芳基亚砜反应的芳基格氏试剂，随后是与ZMF6复分解的第二步， 其中Z是金属或金属状阴离子，M是锑，砷或磷，优选使用铵盐并在非水溶剂中进行。

    Method for making diaryliodonium polyhalometalloid salts
    4.
    发明授权
    Method for making diaryliodonium polyhalometalloid salts 失效
    制备二芳基碘多卤代金属盐的方法

    公开(公告)号：US4329300A

    公开(公告)日：1982-05-11

    申请号：US163725

    申请日：1980-06-27

    Applicant: James V. Crivello ,  Julia H. Lam

    Inventor： James V. Crivello ,  Julia H. Lam

    IPC: C07C25/18 ,  C07F9/68 ,  C07F9/06 ,  C07F9/92

    CPC classification number: C07C25/18

    Abstract: A method is provided for making certain diaryliodonium salt photoinitiators, based on the initial formation of diaryliodonium perchlorate which is formed from a diaryliodonium bisulfate precursor. The diaryliodonium perchlorate is then reacted with a counter ion source, such as an alkali metal hexafluoro metalloid salt, to produce the desired diaryliodonium salt, which can be used as a photoinitiator. The iodonium salt photoinitiators made by the method of the present invention can be used to effect the cure of a variety of cationically polymerizable organic materials, such as epoxy resins.

    Abstract translation: 基于由二芳基碘鎓硫酸氢盐前体形成的高氯酸二芳基碘鎓的初步形成，提供了制备某些二芳基碘盐光引发剂的方法。 然后将高碘酸二芳基碘与抗衡离子源（例如碱金属六氟类准金属盐）反应，以产生可用作光引发剂的所需二芳基碘鎓盐。 通过本发明的方法制备的碘鎓盐光引发剂可用于实现各种阳离子聚合有机材料如环氧树脂的固化。

    P, As, and Sb hexafluoride onium salts as photoinitiators
    5.
    发明授权
    P, As, and Sb hexafluoride onium salts as photoinitiators 失效
    P，As和Sb六氟鎓盐作为光引发剂

    公开(公告)号：US4250311A

    公开(公告)日：1981-02-10

    申请号：US137831

    申请日：1980-04-07

    Applicant: James V. Crivello

    Inventor： James V. Crivello

    IPC: C07F9/90 ,  C08G59/68 ,  G03F7/029 ,  C07F9/06 ,  C07F9/68

    CPC classification number: G03F7/029 ,  C07F9/902 ,  C08G59/68

    Abstract: Halogen onium salts, and onium salts of Group VA and V1A elements having an MF.sub.6.sup.- anion, where M is selected from P, As and Sb, have been found to exhibit unusual activity under ultraviolet light. These onium salts can be employed as cationic photoinitiators when used with a variety of organic resins and cyclic organic compounds.

    Abstract translation: 已经发现，在紫外光下，具有M，选自P，As和Sb的具有MF6-阴离子的组VA和V1A元素的卤素鎓盐和鎓盐呈现异常的活性。 当与各种有机树脂和环状有机化合物一起使用时，这些鎓盐可用作阳离子光引发剂。

    Method for making diaryliodonium salts
    6.
    发明授权
    Method for making diaryliodonium salts 失效
    制备二芳基碘鎓盐的方法

    公开(公告)号：US4238394A

    公开(公告)日：1980-12-09

    申请号：US956024

    申请日：1978-10-30

    Applicant: James V. Crivello ,  Julia H. W. Lam

    Inventor： James V. Crivello ,  Julia H. W. Lam

    IPC: C07C25/18 ,  C07D207/44 ,  C07D207/452 ,  C07F9/68 ,  C07F9/02 ,  C07F9/22

    CPC classification number: C07D207/452 ,  C07C25/18

    Abstract: A method is provided for making certain diaryliodonium salt photoinitiators, based on the initial formation of a diaryliodonium bisulfate. Methylene chloride is substituted for acetic acid during the reaction between potassium iodate and benzene in the presence of acetic anhydride and sulfuric acid. The diaryliodonium bisulfate is then reacted with a counterion source, such as a metal salt, to produce the desired diaryliodonium salt which can be used as a photoinitiator. The iodonium salt photoinitiators made by the method of the present invention can be used to make UV curable compositions.

    Abstract translation: 基于最初形成二芳基碘鎓硫酸氢盐制备某些二芳基碘盐光引发剂的方法。 在乙酸酐和硫酸存在下，在碘酸钾与苯之间的反应过程中，二氯甲烷代替乙酸。 然后将二芳基碘鎓硫酸氢盐与抗衡离子源如金属盐反应，以产生可用作光引发剂的所需二芳基碘鎓盐。 通过本发明的方法制备的碘鎓盐光引发剂可用于制备可UV固化的组合物。

    Organic arsenic compound for creosote fortification
    7.
    发明授权
    Organic arsenic compound for creosote fortification 失效
    有机化合物用于爆炸性强化

    公开(公告)号：US3822137A

    公开(公告)日：1974-07-02

    申请号：US37927073

    申请日：1973-07-16

    Applicant: KOPPERS CO INC

    Inventor： KEMP W

    IPC: C07F9/68 ,  C09D3/24

    CPC classification number: C07F9/68

    Abstract: 5-ARSA-4,6-DIOXACYCLOOCT-5-YL)-

    BIS(1-((HO-CH(-CH3)-CH2-)2-N-(CH2)2-),3,7-DI(H3C-)-1-AZA-

    A WOOD PRESERVATIVE COMPOSITION COMPRISED OF CREOSOTE IN WHICH IS DISSOLVED THE NOVEL ARSENIC-CONTAINING COMPOUND 1- (BIS(E - HYDROXYPROPYL)NITRILOETHYLENE)-5ARSA-1-AZA-4,6-DIOXACYCLOOCTYL AS-ETHER WHOSE STRUCTURE IS

    2,6,7-trioxa-1-arsabicyclo{8 2.2.2{9 octane compounds
    8.
    发明授权
    2,6,7-trioxa-1-arsabicyclo{8 2.2.2{9 octane compounds 失效
    2,6,7-TRIOXA-1-ARSABICYCLO {8 2.2.2 {9 OCTANE COMPOUNDS

    公开(公告)号：US3621044A

    公开(公告)日：1971-11-16

    申请号：US3621044D

    申请日：1969-04-24

    Applicant: GULF RESEARCH DEVELOPMENT CO

    Inventor： DEFFNER JOHN F

    IPC: C07F9/68 ,  C07F9/78 ,  A01N9/00 ,  A01N9/24

    CPC classification number: C07F9/68

    Abstract: Novel derivatives of 2,6,7-trioxa-l-arsabicyclo( 2.2.2)octane are useful as pesticides. The compounds are represented by the general formula

    WHEREIN Z can be alkyl, aryl, aralkyl, alkaryl, cycloalkyl, alkoxy, aryloxy, acyl, acyloxy, acyloxymethyl, benzoxymethyl, amino, nitro, nitrobenzoxymethyl, ammonium nitrobenzoate and chrysanthemumoxymethyl. Examples include 4-PROPYL-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-NITRO-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-AMINO-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-ACETOXYMETHYL-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-BENZOXYMETHYL-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-(P-NITROBENZOXYMETHYL)-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 4-CHRYSANTHEMUMOXYMETHYL-2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTANE 2,6,7-TRIOXA-1-ARSABICYCLO(2.2.2)OCTYL-4-AMMONIUM PNITROBENZOATE.

    LITHIUM SALT
    10.
    发明申请
    LITHIUM SALT 有权
    盐酸盐

    公开(公告)号：US20100010249A1

    公开(公告)日：2010-01-14

    申请号：US12377716

    申请日：2007-09-13

    Applicant: Tatsuo Fujinami ,  Ruoyuan Tao ,  Masaki Matsui

    Inventor： Tatsuo Fujinami ,  Ruoyuan Tao ,  Masaki Matsui

    IPC: C07F9/68 ,  C07F5/02 ,  C07F7/02 ,  C07F7/30 ,  C07F9/06

    CPC classification number: C07F5/022 ,  H01M10/052 ,  H01M10/0568 ,  H01M2300/0025

    Abstract: The principal object of the invention is to provide a lithium salt having excellent ion conductivity. The invention solves the problem by providing a lithium salt having a structure represented by the general formula (1): in which “M” represents B, Si, Ge, P, As or Sb; “X” represents the valence of “M”; “R1” represents —CmH2m— whereupon “m” is an integer of 1 to 4; “R2” represents —CkH2k+1 whereupon “k” is an integer of 1 to 8; and “n” represents 0 to 12.

    Abstract translation: 本发明的主要目的是提供具有优异离子传导性的锂盐。 本发明通过提供具有由通式（1）表示的结构的锂盐来解决该问题：其中“M”表示B，Si，Ge，P，As或Sb; “X”表示“M”的化合价; “R1”表示-CmH2m，其中“m”为1至4的整数; “R2”表示-CkH2k + 1，因此“k”为1〜8的整数， “n”表示0〜12。

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