Integrated pressure oxidative leach of copper sulphidic feed with copper heap leach

    公开(公告)号:US11584975B1

    公开(公告)日:2023-02-21

    申请号:US17458203

    申请日:2021-08-26

    摘要: An integrated pressure leaching, heap leaching process for recovering copper from sulphidic feed containing iron, arsenic, and copper. Aqueous feed slurry of the sulphidic feed is pressure oxidized to form a liquid phase containing free sulphuric acid and aqueous copper sulphate, and to precipitate arsenic as solid iron arsenic compounds. Treated slurry is withdrawn from the pressure vessel and the liquid phase is separated from the solids. Copper is recovered from the separated liquid phase and generates a solution enriched in acid and depleted in copper. At least a portion of this solution is neutralized in a copper heap leach to produce a PLS containing copper and reduced in acid. At least a portion of the heap leach PLS is neutralized to produce a solution further reduced in acid, and solids containing copper precipitates, followed by a liquid solid separation.

    Method for whole component microwave fast digestion and precious metal extraction from ionic liquid of waste circuit board

    公开(公告)号:US20220267879A1

    公开(公告)日:2022-08-25

    申请号:US17743385

    申请日:2022-05-12

    摘要: The invention discloses Method for whole component microwave fast digestion and precious metal extraction from ionic liquid of waste circuit board, and belongs to the field of hydrometallurgy. Based on the theory that microwaves can directly penetrate through a leaching medium to directly heat a circuit board, microwave-assisted leaching can reinforce mass transfer and heat transfer in the traditional leaching process, the leaching time is greatly shortened, and the leaching efficiency is improved. Before leaching, a waste circuit board does not need to be smashed, and environmental protection is achieved while energy is saved. The temperature rising process and reaction time of the reaction can be controlled, the whole process is conducted under the airtight condition, heat loss in the leaching process is avoided, the valuable leaching rate is high, the selectivity is high, and efficient leaching of valuable metal can be achieved. Precious metal leachate is extracted through imidazolium ionic liquid, the selectivity of the imidazolium ionic liquid to gold is high, and the co-extraction phenomenon of gold, nickel, copper and other ions is avoided. The method for extracting the precious metal leachate through ionic liquid is a green and clean recycling method, and the overall recycling rate of gold, nickel and copper can reach 99% or above

    METHOD FOR RECOVERING GOLD AND COPPER FROM ELECTRONIC COMPONENTS

    公开(公告)号:US20220136080A1

    公开(公告)日:2022-05-05

    申请号:US17434224

    申请日:2020-02-21

    发明人: Gaetano FRISI

    摘要: A method for recovering gold from electronic components includes a first macro-step of dissolving gold and copper from the electronic components using an aqueous solution comprising HNO3 concentrated in a percentage varying from 28% to 38% and concentrated HCl in a percentage varying from 15% to 25%. A second macro-step includes adding KOH to the obtained solution to bring it to a pH between 0.5 and 0.9. A third macro-step includes adding to the solution obtained in the second macro-step an amount of ascorbic acid dissolved in water equal to the amount of gold hypothetically present in a sample of the first macro-step, multiplied by a factor ranging between 1.5 and 3, causing precipitation of gold, which is separated from the solution and made available in powder form in a fourth macro-step.

    BATTERY RECYCLING PROCESS
    7.
    发明申请

    公开(公告)号:US20220017989A1

    公开(公告)日:2022-01-20

    申请号:US17414831

    申请日:2019-12-03

    摘要: A method for the recovery of metals from a feed stream containing one or more value metals and lithium, the method comprising: subjecting the feed stream to a sulphuric acid leach to form a slurry comprising a pregnant leach solution of soluble metal salts and a solid residue; separating the pregnant leach solution and the solid residue; subjecting the pregnant leach solution to one or more separate solvent extraction steps, wherein each solvent extraction step recovers one or more value metals from the pregnant leach solution, the remaining pregnant leach solution comprising lithium; and recovery of lithium from the pregnant leach solution.

    System for use in producing a metal ion suspension and process of using same

    公开(公告)号:US11193184B2

    公开(公告)日:2021-12-07

    申请号:US16283605

    申请日:2019-02-22

    IPC分类号: C22B15/00 C22B3/22 C22B3/02

    摘要: Provided herein is a system for producing suspensions comprising soluble metal ions. The system comprises a basket to hold a metal load comprising a permeable floor so as to allow a solution to come into contact with the metal load. The system further comprises a vessel within which the solution and the basket may be maintained while metal ions are leached from the metal load into the solution. Some embodiments of the present disclosure pertain to a system used to produce a suspension comprising copper ions. Additionally, provided herein are methods of using the system to produce suspensions comprising soluble metal ions. Some embodiments of the present disclosure pertain to methods of making suspensions comprising copper ions. The resultant suspensions comprising metal ions may be further modified to supply a pharmaceutically acceptable treatment.

    COUNTERCURRENT PROCESS FOR RECOVERING HIGH PURITY COPPER SULFATE VALUES FROM LOW GRADE ORES

    公开(公告)号:US20210347651A1

    公开(公告)日:2021-11-11

    申请号:US16994625

    申请日:2020-08-16

    摘要: A method for extracting copper values from a low grade copper ore feedstock is provided. The method includes (a) providing an ore feedstock of a copper oxide ore; (b) subjecting the ore to at least one process selected from the group consisting of primary crushing processes and secondary crushing processes; (c) subjecting the ore feedstock to high pressure grinding roll crushing, thereby obtaining a crushed ore; (d) subjecting the crushed ore to acid curing, thereby obtaining a cured ore; (e) subjecting the cured ore to vat or heap leaching, thus yielding a leachate; (f) passing the leachate through a first ion exchange resin which is selective to base metals plus copper, thereby removing a portion of the copper values from the leachate and yielding a first loaded resin and a first treated leachate; (g) stripping base metals plus copper values from the first loaded resin with a first stripping solution, thereby yielding a base metals plus copper-loaded stripping solution; (h) selectively extracting copper values from the copper-loaded stripping solution via solvent extraction, thereby obtaining an extract and a raffinate; and (i) crystallizing a copper salt from the extract, thereby obtaining a crystallized copper salt.