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公开(公告)号:US12123086B2
公开(公告)日:2024-10-22
申请号:US17185521
申请日:2021-02-25
Applicant: BIOTRONIK AG
Inventor: Heinz Mueller , Peter Uggowitzer , Joerg Loeffler
CPC classification number: C22F1/06 , A61F2/82 , A61L27/047 , A61L27/58 , A61L31/022 , A61L31/148 , C22C23/02
Abstract: A method for producing a magnesium alloy having improved mechanical and electrochemical properties. The method includes generating a high-purity magnesium by vacuum distillation. A billet of the alloy is generated by synthesis of the high-purity magnesium with 2.0 to 10.0% by weight Al, the remainder being magnesium containing impurities, which promote electrochemical potential differences and/or the formation of precipitations and/or intermetallic phases, in a total amount of no more than 0.0063% by weight of Fe, Si, Mn, Co, Ni, Cu, Zr, Y, Sc or rare earths having the ordinal numbers 21, 57 to 71 and 89 to 103, Be, Cd, In, Sn and/or Pb as well as P, wherein the matrix of the alloy includes intermetallic phases formed of Mg and Al. The alloy is homogenized by annealing at a temperature between 150° C. and 450° C. The homogenized alloy is formed in the temperature range between 200° C. and 400° C.
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公开(公告)号:US20240344189A1
公开(公告)日:2024-10-17
申请号:US18752536
申请日:2024-06-24
Applicant: Terves, LLC
Inventor: Brian P. Doud , Nicholas J. Farkas , Andrew Sherman
Abstract: A castable, moldable, and/or extrudable structure using a metallic primary alloy. One or more additives are added to the metallic primary alloy so that in situ galvanically-active reinforcement particles are formed in the melt or on cooling from the melt. The composite contains an optimal composition and morphology to achieve a specific galvanic corrosion rate in the entire composite. The in situ formed galvanically-active particles can be used to enhance mechanical properties of the composite, such as ductility and/or tensile strength. The final casting can also be enhanced by heat treatment, as well as deformation processing such as extrusion, forging, or rolling, to further improve the strength of the final composite over the as-cast material.
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公开(公告)号:US11969519B1
公开(公告)日:2024-04-30
申请号:US18324388
申请日:2023-05-26
Applicant: Bioretec Oy
Inventor: Timo Lehtonen , Kimmo Lähteenkorva , Anna-Maija Haltia , Christopher Stahle
IPC: A61L27/00 , A61F2/28 , A61F2/30 , A61L27/04 , A61L27/44 , A61L27/58 , A61L31/02 , A61L31/14 , C22C1/02 , C22C23/00 , C22F1/06
CPC classification number: A61L27/047 , A61L27/042 , A61L27/446 , A61L27/58 , A61L31/022 , A61L31/148 , C22C1/02 , C22C23/00 , C22F1/06 , A61L2420/02
Abstract: The present application provides an orthopedic implant or a part thereof, comprising biodegradable magnesium alloy comprising magnesium and Ca in the range of 0.550-0.700 wt %, Zn in the range of 0.400-0.700 wt %, and Fe 50 ppm or less, the biodegradable magnesium alloy consisting of two phases comprising a first phase comprising magnesium and Zn and a second phase less noble than the first phase, the second phase comprising Mg2Ca precipitates larger than nano-sized. The present application also provides a method for preparing the biodegradable magnesium alloy, a method for preparing the orthopedic implant or the part thereof, and a method for treating a subject in need of therapy for a medical condition of a bone.
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公开(公告)号:US20240026499A1
公开(公告)日:2024-01-25
申请号:US18224247
申请日:2023-07-20
Applicant: Ohio State Innovation Foundation , Terves, Inc.
Inventor: Alan Luo , Joshua Caris , Thomas Avey
Abstract: Disclosed herein are magnesium alloys and methods of making and use thereof. For example, disclosed herein are magnesium alloys comprising: from 0 to 1.5 wt. % Zn; from 0 to 1.5 wt. % Al; less than 0.2 wt. % Ca; from 0.2 to 0.4 wt. % Ce; from 0.1 to 0.8 wt. % Mn; and the balance comprising Mg. In some examples, the magnesium alloy comprises less than 1 wt. % Zn. In some examples, the magnesium alloy comprises less than 1 wt. % Al. In some examples, the magnesium alloy exhibits substantially no incipient melting when extruded with a ram speed of from 1.00 to 10.00 ipm. In some examples, the magnesium alloy is substantially free of a Mg2Ca phase, an AlCaMg phase, an Al2Ca phase, a Ca2Mg6Zn3 phase, or a combination thereof. In some examples, the magnesium alloy is substantially free of a Mg2Ca phase.
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公开(公告)号:US20230416880A1
公开(公告)日:2023-12-28
申请号:US18038928
申请日:2020-11-30
Applicant: SANKYO TATEYAMA, INC.
Inventor: Yasunobu MATSUMOTO , Masayoshi OGAWA , Tomoya OZASA , Kazunori SHIMIZU , Akira NAKAGAWA , Shun KANITANI
Abstract: An Mg alloy is provided the degradation of which is promoted by forming and crystallizing an Al—Mn—Ni system intermetallic compound containing Ni together with the metals included in a magnesium alloy, and thereby dispersing Ni in the magnesium alloy.
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公开(公告)号:US20230381845A1
公开(公告)日:2023-11-30
申请号:US17872766
申请日:2022-07-25
Applicant: GM GLOBAL TECHNOLOGY OPERATIONS LLC
Inventor: Henry ZHAN , Congjie WANG
CPC classification number: B21C23/002 , C22C23/00 , C22F1/06
Abstract: The present disclosure provides a method of forming an extruded billet from a coarse-grained magnesium alloy billet. The method includes extruding the coarse-grained magnesium alloy biller at temperatures greater than or equal to about 300° C. to less than or equal to about 360° C. to from the extruded billet. The coarse-grained magnesium alloy billet has an average grain size greater than or equal to about 800 μm, and has a low aluminum content. The coarse-grained magnesium alloy billet includes greater than or equal to about 0.5 wt. % to less than or equal to about 3 wt. % of aluminum. The extruded billet may have a plurality of twins with lenticular morphology, which occupies an area fraction greater than or equal to about 20% of a total area of the extruded billet.
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公开(公告)号:US11813653B2
公开(公告)日:2023-11-14
申请号:US17944218
申请日:2022-09-14
Applicant: North University of China
Inventor: Zhimin Zhang , Jianmin Yu , Zhen Wang , Zhe Cheng , Mei Cheng
CPC classification number: B21D22/022 , C22F1/06
Abstract: The present disclosure discloses a method for preparing large-size rare earth magnesium alloy with high-performance ingots by short process severe plastic deformation. When in use, the pushing cylinder moves upward, and the back pressure plate is adjusted to the outlet of the extrusion deformation area. After the male mold stroke is completed, the recoverable discard block fills the extrusion deformation area, and the upsetting extrusion deformation is completed. Then, the pushing cylinder drives the back pressure plate to remove from the lower part of the lower mold cavity downward, and the recoverable discard block has been broken due to the high pressure. Then, the extruded blank and residual block powder are taken out from the lower part of the lower mold cavity, restored into a plate shape for the next use. The present disclosure can solve the tail shrinking phenomenon, save materials and increase the strengthening effect.
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公开(公告)号:US11795533B2
公开(公告)日:2023-10-24
申请号:US15931104
申请日:2020-05-13
Applicant: QILU UNIVERSITY OF TECHNOLOGY , ADVANCED MATERIALS INSTITUTE, SHANDONG ACADEMY OF SCIENCES
Inventor: Jixue Zhou , Yunteng Liu , Dongqing Zhao , Baichang Ma , Meifang Wang , Peiliang Li , Cong Liu , Shouqiu Tang
Abstract: A heat-resistant and soluble magnesium alloy, and a preparation method having an elemental composition at the following atomic percentage: Lu 0.10% to 8.00%, Ce 0.001 to 0.05%, Al 0.10% to 0.60%, Ca 0.001% to 0.50%, Cu 0.01% to 1.00%, Ni 0.01% to 1.00%, impurity elements
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公开(公告)号:US11773472B2
公开(公告)日:2023-10-03
申请号:US16954377
申请日:2018-12-21
Applicant: POSCO CO., LTD
Inventor: Jun Ho Park , Hyun Bom Lee , Jae Joong Kim , Oh-Duck Kwon
CPC classification number: C22C23/02 , B21B3/003 , C21D8/0273 , C22F1/06
Abstract: The present invention relates to a magnesium alloy sheet and a manufacturing method thereof. In detail, the magnesium alloy sheet includes 0.5 to 3.5 wt % of Al, 0.5 to 1.5 wt % of Zn, 0.1 to 1.0 wt % of Ca, 0.01 to 1.0 wt % of Mn, a remainder of Mg, and other inevitable impurities with respect to an entire 100 wt % of a magnesium alloy sheet, wherein an average crystal grain size of the magnesium alloy sheet is 3 to 15 μm, the magnesium alloy sheet includes a stringer, and a length of the stringer in a rolling direction (RD) is equal to or less than the maximum value of 50 μm.
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公开(公告)号:US11766713B2
公开(公告)日:2023-09-26
申请号:US17481641
申请日:2021-09-22
Applicant: GM Global Technology Operations LLC
Inventor: Henry Zhan , Congjie Wang
Abstract: A method to form a magnesium article includes: heating materials including magnesium, aluminum, manganese and tin in a furnace to create an alloy having a composition of; the magnesium in an amount greater than or equal to 90% by weight of the materials; the aluminum ranging between approximately 2.0% up to approximately 4.0% by weight of the materials; the manganese ranging between approximately 0.43% up to approximately 0.6% by weight of the materials; and the tin ranging between approximately 1% up to approximately 3% by weight of the materials; chill casting the alloy to create a cast billet; and heating the cast billet at a temperature ranging from approximately 380° C. up to approximately 420° C. and maintaining the temperature for a time period between approximately 4 hours to 10 hours to homogenize element distribution.
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