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1.发明授权公开(公告)号：US12018380B2
公开(公告)日：2024-06-25
申请号：US17433312
申请日：2019-12-18
摘要： Metallic substrate treatment methods and articles comprising a phosphonate functionalized layer are provided. The method comprises contacting a metallic substrate comprising at least one of aluminum and an aluminum alloy with a fluid to form a phosphonate functionalized layer on at least a region of the metallic substrate. The fluid comprises at least one of a phosphonate containing acid and a derivative thereof. At least one of the phosphonate containing acid and the derivative thereof comprises a pKa of a first acidic proton. The fluid comprises a pH at least 0.5 pH value greater than the pKa of the first acidic proton. The article comprises a metallic substrate comprising aluminum or an aluminum alloy and a phosphonate functionalized layer on at least a region of the metallic substrate.
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公开(公告)号：US11987725B2
公开(公告)日：2024-05-21
申请号：US15838614
申请日：2017-12-12
申请人： THE BOEING COMPANY
IPC分类号： C09D5/08 , C09D1/00 , C09D5/00 , C09D7/20 , C09D7/40 , C09D7/63 , C09J5/02 , C23C18/04 , C23C18/12 , C23C22/73
CPC分类号： C09D5/086 , C09D1/00 , C09D5/00 , C09D5/08 , C09D7/20 , C09D7/40 , C09D7/63 , C09J5/02 , C23C18/04 , C23C18/1216 , C23C18/122 , C23C18/1241 , C23C18/1254 , C23C22/73
摘要： The present disclosure provides sol-gels, sol-gel films and substrates, such as vehicle components, having a sol-gel film disposed thereon. At least one sol-gel is the reaction product of an organosilane, a metal alkoxide, an acid stabilizer, and an organic solvent, the sol-gel having about 10 wt % or less water content based on the total weight of the sol-gel. At least one vehicle component comprises a sol-gel coating system, comprising a metal substrate and a sol-gel disposed on the metal substrate, and the sol-gel is the reaction product of an organosilane, a metal alkoxide, an acid stabilizer, and an organic solvent, the sol-gel having about 10 wt % or less water content based on the total weight of the sol-gel.
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公开(公告)号：US20240150582A1
公开(公告)日：2024-05-09
申请号：US18415235
申请日：2024-01-17
IPC分类号： C09D5/00 , C09D1/00 , C09D5/16 , C09D7/40 , C09D7/65 , C09D127/18 , C23C22/05 , C23C22/73 , F28F13/04 , F28F13/18
CPC分类号： C09D5/002 , C09D1/00 , C09D5/1618 , C09D5/1681 , C09D7/65 , C09D7/70 , C09D127/18 , C23C22/05 , C23C22/73 , F28F13/04 , F28F13/185 , F28F13/187 , F28F2245/04
摘要： The invention relates generally to liquid-repellent coatings, and in particular, to porous liquid-repellent coatings, a method of preparing the porous liquid-repellent coatings, and a method of characterizing a porous surface for the liquid-repellent coatings. The invention further relates to a porous liquid-repellent coating comprising a porous layer of a transition metal oxide and/or hydroxide and a layer of a liquid-repellent compound deposited onto the porous layer of the transition metal oxide and/or hydroxide, wherein the porous layer of the transition metal oxide and/or hydroxide is comprised of a plurality of surface pores of varying angles with an average angle that is re-entrant.
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公开(公告)号：US20240060187A1
公开(公告)日：2024-02-22
申请号：US18386772
申请日：2023-11-03
IPC分类号： C23C22/66 , C23F1/20 , C23C22/76 , B41N1/08 , B05D3/10 , C23C22/78 , C23F11/167 , C23C22/56 , C09D5/08 , C23C22/73 , C09D5/12
CPC分类号： C23C22/66 , C23F1/20 , C23C22/76 , B41N1/083 , B05D3/102 , C23C22/78 , C23F11/167 , C23C22/56 , C09D5/08 , C23C22/73 , C09D5/12
摘要： Described herein is a continuous coil pretreatment process used to treat the surface of an aluminum alloy sheet or coil for subsequent deposition of an acidic organophosphorus compound. The process can include applying a cleaner to a surface of an aluminum sheet or a coil; etching the surface of the aluminum sheet or the coil with an acidic solution; rinsing the surface of the aluminum sheet or the coil with deionized water; applying to the surface of the aluminum sheet or the coil a solution of an acidic organophosphorus compound; rinsing the surface of the aluminum sheet or the coil with deionized water; and drying the surface of the aluminum sheet or the coil.
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公开(公告)号：US11505722B2
公开(公告)日：2022-11-22
申请号：US15837058
申请日：2017-12-11
申请人： THE BOEING COMPANY
IPC分类号： C09D5/08 , C09D185/00 , B64D45/00 , C09D5/00 , C23C18/12 , C09J9/00 , C09J11/06 , B01J13/00 , C09J5/02 , C09D1/00 , C23C22/73
摘要： The present disclosure provides methods for forming sol-gels, sol-gel films and substrates, such as vehicle components, having a sol-gel film disposed thereon. At least one method of forming a sol-gel includes mixing a metal alkoxide, an acid stabilizer, and an organic solvent to form a first mixture having about 10 wt % or less water content based on the total weight of the first mixture. The method includes mixing an organosilane with the first mixture to form a second mixture having about 10 wt % or less water content based on the total weight of the second mixture.
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公开(公告)号：US11453948B2
公开(公告)日：2022-09-27
申请号：US16538711
申请日：2019-08-12
发明人： Betar Gallant , Mingfu He , Rui Guo
IPC分类号： H01M10/0562 , H01M10/0525 , C23C22/73 , C23C22/78
摘要： Articles and methods related to passivation layers on alkali metals are generally described.
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公开(公告)号：US20220267907A1
公开(公告)日：2022-08-25
申请号：US17626298
申请日：2020-07-07
摘要： Composition, characterized in that: —it comprises, in a solution of demineralized water: between 10 and 80, preferably between 15 and 20, more preferably 17, g/l of a composition of phosphoric acid H3PO4, and between 2 and 15, preferably between 4 and 8, more preferably 6, g/l of a composition of potassium permanganate KMnO4, —the weight ratio H3PO4/KMnO4 is between 1.5 and 10, preferably between 1.8 and 5, mote preferably equal to 2.8, —said composition has a pH between 2.4 and 3, preferably 2.5.
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公开(公告)号：US20220127745A1
公开(公告)日：2022-04-28
申请号：US17077181
申请日：2020-10-22
发明人： Lei Chen , James O. Hansen
摘要： A sealing process includes impregnating an oxide layer of an anodized metal with a corrosion inhibitor by contacting the oxide layer with a first corrosion inhibitor solution at a first temperature and sealing the impregnated oxide layer of an anodized metal by contacting the impregnated oxide layer with a second corrosion inhibitor solution at a second temperature, wherein the first corrosion inhibitor solution has a corrosion inhibitor concentration greater than the second corrosion inhibitor solution and the first temperature is less than the second temperature.
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9.发明申请公开(公告)号：US20210340676A1
公开(公告)日：2021-11-04
申请号：US17282665
申请日：2019-10-08
申请人： Chemetall GmbH , Rhodia Operations
IPC分类号： C23C22/18 , C23C22/83 , C23C22/78 , C23C22/73 , C09D153/00
摘要： Described herein is a method for treatment of at least one surface of a metal containing substrate including at least contacting the surface with an aqueous acidic Ni-free composition (A) including at least zinc cations, manganese cations, and phosphate anions to form a conversion coating on the surface and contacting the formed coating with an aqueous Ni-free composition (B) including one or more linear polymers (P) containing at least vinyl phosphonic acid, (meth)acrylic acid, and hydroxyethyl- and/or hydroxypropyl (meth)acrylate in form of their polymerized monomeric units. Also described herein is the composition (B), a master batch to produce the composition (B), a kit-of-parts including both compositions (A) and (B), a kit-of-parts including respective master batches to produce both compositions (A) and (B), and a coated substrate obtainable by the method described herein.
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公开(公告)号：US20210198788A1
公开(公告)日：2021-07-01
申请号：US17125539
申请日：2020-12-17
申请人： ENTEGRIS, INC.
发明人： Carlo WALDFRIED , Bryan C. HENDRIX
摘要： Described are metal bodies made of magnesium-containing metal and having a magnesium fluoride surface passivation region formed at a surface of the body, as well as methods of forming a magnesium fluoride surface passivation region at a surface of a metal body, and uses for the bodies.
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