PROCESSES FOR PRODUCING GRANULAR COPPER

    公开(公告)号:US20220402030A1

    公开(公告)日:2022-12-22

    申请号:US17811673

    申请日:2022-07-11

    摘要: Processes for producing copper granules on a surface of a reducing metal. The process can include contacting the reducing metal with an aqueous solution comprising a copper(II) salt and a halide. The molar ratio of the halide to the copper(II) in the copper (II) salt can be at least about 3:1. The granular copper can be produced on a surface of the reducing metal, and is optionally removed from the surface of the reducing metal by shaking, washing, and/or brushing, and/or optionally with stirring and/or circulating of the aqeuous solution.

    Method for preparing nickel nanopowders and method for making nickel nanopowders into paste

    公开(公告)号:US11090722B2

    公开(公告)日:2021-08-17

    申请号:US16608951

    申请日:2018-04-27

    申请人: SOLUETA CO., LTD.

    IPC分类号: B22F9/20 B22F1/00 H01G4/008

    摘要: Provided is a method for making nickel nanopowders into paste including: (a) preparing a nickel oxide configured in the form of an oxide; (b) preparing nano-sized nickel oxide nanopowders by pulverizing the nickel oxide; (c) a step of drying the nickel oxide nanopowders; (d) a step of preparing natural metal nickel nanopowders by preparing the nickel oxide nanopowders as the natural metal nickel nanopowders through a reduction process in a hydrogen atmosphere and heat-treating the same at the same time; (e) a step of simultaneously performing a step of crushing the natural metal nickel nanopowders prepared by the heat treatment and a nanopowder oxidation preventing coating step of forming an oxidation preventing film on the natural metal nickel nanopowders with an additive; and (f) a step of making the natural metal nickel nanopowders, which have been simultaneously subjected to the crushing and coating steps, into paste.

    Methods for Producing Metal Powders
    6.
    发明申请

    公开(公告)号:US20200023440A1

    公开(公告)日:2020-01-23

    申请号:US16282385

    申请日:2019-02-22

    IPC分类号: B22F9/24 B22F9/20 C22B5/04

    摘要: A method for producing a metal powder includes maintaining molten reducing metal in a sealed reaction vessel that is free of added oxygen and water, establishing a vortex in the molten reducing metal, introducing a metal halide into the vortex so that the molten reducing metal is in a stoichiometric excess to the metal halide, thereby producing metal particles and salt, removing unreacted reducing metal, removing the salt, and recovering the metal powder. The molten reducing metal can be a Group I metal, a Group II metal, or aluminum.

    PRODUCING TITANIUM ALLOY MATERIALS THROUGH REDUCTION OF TITANIUM TETRACHLORIDE

    公开(公告)号:US20190270140A1

    公开(公告)日:2019-09-05

    申请号:US16343462

    申请日:2017-10-20

    IPC分类号: B22F9/24 B22F9/20 B22F1/00

    摘要: Processes are provided for producing a titanium alloy material, such as Ti—Al alloys. In one embodiment, the process includes: heating an input mixture to a preheat temperature with the input mixture including aluminum, optionally, AlCl3, and, optionally ally, one or more alloying element halide; introducing TiCl4 to the input mixture at the first reaction temperature such that substantially all of the Ti4+ in the TiCl4 is reduced to Ti3+; thereafter, heating to a second reaction temperature such that substantially all of the Ti3+ is reduced to Ti2+ to form an intermediate mixture (e.g., a Ti2+ salt); and introducing the intermediate mixture into a reaction chamber at a disproportionation temperature reaction to form the titanium alloy material from the Ti2+ via a disproportionation reaction.