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    METHOD FOR PRODUCING POLYALKYLENE GLYCOL DERIVATIVE HAVING AMINO GROUP AT END
    2.
    发明申请
    METHOD FOR PRODUCING POLYALKYLENE GLYCOL DERIVATIVE HAVING AMINO GROUP AT END 审中-公开

    公开(公告)号：US20190322688A1

    公开(公告)日：2019-10-24

    申请号：US16454785

    申请日：2019-06-27

    申请人： Shin-Etsu Chemical Co., Ltd.

    发明人： Yuki Suka ,  Yuji Harada ,  Takeru Watanabe ,  Shiori Nonaka

    IPC分类号： C07F7/08 ,  C08G65/333 ,  C07F7/10 ,  C08G65/26 ,  C08G65/12

    摘要： A method simply produces a narrowly distributed and high-purity polyalkylene glycol derivative having an amino group at an end without using a heavy metal catalyst. A method for producing a polyalkylene glycol derivative having an amino group at the end by reacting a compound represented by the general formula (V) with an alkylene oxide, then reacting a reaction product with an electrophile represented by the general formula (I), and deprotecting the obtained product without using a heavy metal: RA3O(RA4O)k−1RA4O−M+  (V) wherein RA3 represents a linear, branched, or cyclic hydrocarbon group having 1 to 20 carbon atoms; RA4 represents an alkylene group having 2 to 8 carbon atoms; k represents an integer of 2 to 5; and M represents an alkali metal; wherein RA1a and RA1b each independently represent a protective group of the amino group, or one of RA1a and RA1b represents H and the other represents a protective group of the amino group, or RA1a and RA1b bind to each other to form a cyclic protective group, and the protective group is deprotectable without using a heavy metal; RA2 represents a linear, branched, or cyclic hydrocarbon group having 1 to 6 carbon atoms; and X represents a leaving group.

    ALKYLENE OXIDE POLYMER PRODUCTION METHOD
    3.
    发明申请
    ALKYLENE OXIDE POLYMER PRODUCTION METHOD 审中-公开

    公开(公告)号：US20180319933A1

    公开(公告)日：2018-11-08

    申请号：US16036580

    申请日：2018-07-16

    申请人： SUMITOMO SEIKA CHEMICALS CO., LTD.

    发明人： Toru Ido ,  Noboru Yamaguchi

    IPC分类号： C08G65/12 ,  C08G65/10 ,  C08G65/26

    CPC分类号： C08G65/12 ,  C08G65/10 ,  C08G65/266

    摘要： Provided is a method to produce an alkylene oxide polymer having a high polymerization degree on an industrial scale and with high reproducibility. The method includes the step of carrying out a polymerization reaction of an alkylene oxide in an inert hydrocarbon solvent in the presence of a zinc catalyst to produce an alkylene oxide polymer. The zinc catalyst is produced by reaction of an organozinc compound with a monohydric alcohol in an amount of 12-fold equivalent or less relative to the amount of the organozinc compound and an aliphatic polyhydric alcohol in an amount of 0.2- to 1.1-fold equivalent relative to the amount of the organozinc compound. The polymerization reaction is carried out under such a condition that the amount of the monohydric alcohol in the polymerization reaction system becomes 0.01-fold equivalent or less relative to the amount of the organozinc compound.

    Method For Cyclically Preparing Polyether Polyol By Using DMC Catalyst
    4.
    发明申请
    Method For Cyclically Preparing Polyether Polyol By Using DMC Catalyst 审中-公开

    公开(公告)号：US20180171073A1

    公开(公告)日：2018-06-21

    申请号：US15513972

    申请日：2016-03-30

    申请人： Huaian Bud Polyurethane Science & Technology Co., Ltd.

    发明人： Weixin Qi ,  Bing Hu ,  Yong Han

    IPC分类号： C08G65/26 ,  C08G65/12

    摘要： The present disclosure discloses a method for preparing a polyether polyol in a continuous reaction cycle. In the method, a low molecular-weight alcohol is polymerized with an alkylene oxide to obtain a low molecular-weight polymer. The low molecular-weight polymer is used as an initiator to react with the alkylene oxide and the low molecular-weight alcohol in the presence of a DMC catalyst and an acid promoter to obtain an intermediate-target polymer. A portion of the intermediate-target polymer is used for producing the target polymer, and the other portion is recycled for reproduction of the intermediate-target polymer. In the present disclosure, no initiator prepared with a base catalyst is used, and thus the loss of material and the discharge of residue and waste water are reduced. The DMC concentration is kept constant in the target polymer during the production such that the dewatering time and induction time are greatly reduced.

    ETHYLENE OXIDE-CONTAINING COPOLYMERS AND METHODS THEREOF
    7.
    发明申请
    ETHYLENE OXIDE-CONTAINING COPOLYMERS AND METHODS THEREOF 审中-公开
    含乙氧基的含氧共聚物及其方法

    公开(公告)号：US20150266997A1

    公开(公告)日：2015-09-24

    申请号：US14734093

    申请日：2015-06-09

    申请人： Dow Global Technologies LLC

    发明人： Abhijit Ghosh-Dastidar ,  Eric P. Wasserman

    IPC分类号： C08G65/12 ,  H01M4/62

    CPC分类号： C08G65/12 ,  C08G65/2654 ,  C08G65/2657 ,  C08G65/3312 ,  C08G2650/58 ,  C08L2205/05 ,  H01M4/621 ,  H01M4/622 ,  H01M10/052 ,  H01M10/0565 ,  H01M2004/021 ,  Y02E60/122

    摘要： The present invention is directed at a binder for a battery electrode comprising an ethylene oxide-containing copolymer including a first monomer of ethylene oxide (EO) and at least one additional monomer selected from an alkylene-oxide that is different from the first monomer of EO, an alkyl glycidyl ether, or a combination thereof; wherein the ethylene oxide-containing copolymer has a weight average molecular weight less than about 200,000 g/mole (e.g., from about 10,000 to about 100,000), the molar fraction of the first monomer of EO (XEO) in the ethylene oxide-containing copolymer is greater than 0.80 (e.g., from about 0.80 to about 0.995), and the ethylene oxide-containing copolymer has a peak melting temperature (Tp), in ° C., for a selected XEO in the range of about 0.80 to about 0.995, which is below a maximum value of Tpmax, at the selected XEO, which is calculated using the equation Tpmax=(60−150 (1−XEO)).

    摘要翻译： 本发明涉及一种用于电池电极的粘合剂，其包含含环氧乙烷的共聚物，其包含环氧乙烷（EO）的第一单体和至少一种选自不同于EO的第一单体的烯化氧的另外的单体 ，烷基缩水甘油醚或其组合; 其中所述含环氧乙烷的共聚物的重均分子量小于约200,000g / mol（例如约10,000至约100,000），所述含环氧乙烷的共聚物中EO（XEO）的第一单体的摩尔分数 大于0.80（例如，约0.80至约0.995），并且对于所选择的XEO，含环氧乙烷的共聚物的峰值熔融温度（Tp）在℃为约0.80至约0.995的范围内， 在选定的XEO下低于Tpmax的最大值，其使用公式Tpmax =（60-150（1-XEO））计算）。

    Organometallic catalyst and preparation thereof
    8.
    发明授权
    Organometallic catalyst and preparation thereof 有权
    有机金属催化剂及其制备方法

    公开(公告)号：US09062155B2

    公开(公告)日：2015-06-23

    申请号：US13945367

    申请日：2013-07-18

    申请人： The University of Sydney

    发明人： Fariba Dehghani ,  Zhong Xia

    IPC分类号： C08G64/30 ,  C07F3/06 ,  C09K3/00 ,  C07C51/41 ,  C08G64/02 ,  C08G64/34 ,  C08G65/12

    CPC分类号： C08G64/302 ,  C07C51/418 ,  C08G64/0208 ,  C08G64/34 ,  C08G65/12 ,  Y02P20/544 ,  C07C55/12

    摘要： The present invention relates to a method for producing an organometallic catalyst and an organometallic catalyst when produced by the method. The method comprises the steps of combining a polycarboxylic acid or anhydride and a metal-oxide, metal-hydroxide or metal-salt with a solvent at a temperature and pressure at which the solvent exists as a supercritical or near-critical fluid. The polycarboxylic acid or anhydride is reacted with the metal-oxide, metal-hydroxide or metal-salt for sufficient time and under sufficient temperature and pressure to produce the organometallic catalyst. The present invention also relates to a process for making a poly(alkylene carbonate) in the presence of a catalytic amount of the organometallic catalyst produced by the method.

    摘要翻译： 本发明涉及通过该方法制备有机金属催化剂和有机金属催化剂的方法。 该方法包括在溶剂作为超临界或近临界流体存在的温度和压力下将多元羧酸或酸酐与金属氧化物，金属氢氧化物或金属盐与溶剂组合的步骤。 使多元羧酸或酸酐与金属氧化物，金属氢氧化物或金属盐反应足够的时间和足够的温度和压力以产生有机金属催化剂。 本发明还涉及在通过该方法制备的催化量的有机金属催化剂的存在下制备聚（碳酸亚烷基酯）的方法。

    PROCESS FOR PRODUCING POLYETHER
    10.
    发明申请
    PROCESS FOR PRODUCING POLYETHER 审中-公开
    生产聚醚的方法

    公开(公告)号：US20120172537A1

    公开(公告)日：2012-07-05

    申请号：US13418842

    申请日：2012-03-13

    申请人： Takeaki ARAI ,  Chitoshi Suzuki

    发明人： Takeaki ARAI ,  Chitoshi Suzuki

    IPC分类号： C08G65/12 ,  C08G18/48 ,  C08G65/26

    CPC分类号： C08G65/2663 ,  C08G18/4866 ,  C08G18/4887 ,  C08G65/2696

    摘要： To provide a process for producing a polyether, which comprises subjecting an alkylene oxide and the like to ring-opening addition polymerization to an initiator in the presence of a double metal cyanide complex catalyst (DMC catalyst), which can be carried out by use of a DMC catalyst at a low concentration, and accordingly the amount of the DMC catalyst remaining in a polyether to be obtained can be reduced.A process for producing a polyether, which comprises subjecting an alkylene oxide and an oxygen-containing heterocyclic compound other than an alkylene oxide, to ring-opening addition polymerization to an initiator having a hydroxy group in the presence of a DMC catalyst, wherein prior to the ring-opening addition polymerization, the DMC catalyst and the initiator are subjected to mixing treatment at a temperature of from 125° C. to 180° C. under an absolute pressure of at most 0.06 MPa for from 10 minutes to 24 hours.

    摘要翻译： 提供一种制备聚醚的方法，其包括在双金属氰化物配合物催化剂（DMC催化剂）的存在下，使烯化氧等进行开环加成聚合，引发剂可以通过使用 低浓度的DMC催化剂，因此可以降低残留在所得聚醚中的DMC催化剂的量。 一种制备聚醚的方法，其包括使环氧烷和除了烯化氧以外的含氧杂环化合物在DMC催化剂的存在下开环加成聚合成具有羟基的引发剂，其中在 开环加成聚合，DMC催化剂和引发剂在125℃至180℃的温度下在绝对压力至多为0.06MPa下进行10分钟至24小时的混合处理。