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发明公开
CN104152953A 磷酸槽电镀铂用的主盐及其合成方法 无效 - 撤回

磷酸槽电镀铂用的主盐及其合成方法
摘要：
本发明公开了磷酸槽电镀铂用的主盐及其合成方法，为新型酸性磷酸槽镀铂用的主盐—磷酸二氢四氨合铂和碱性磷酸槽镀铂用的主盐—磷酸四氨合铂的结构和合成方法。合成经过如下步骤：磷酸二氢银沉淀二氯四氨合铂的氯离子合成磷酸二氢四氨合铂；磷酸银沉淀二氯四氨合铂的氯离子合成磷酸四氨合铂。合成方法具有流程短、反应速度快、产率高(＞98.0％)、产品纯度>99.0％的优点，适合于批量合成。
摘要（英）：

The invention discloses main salt for phosphoric acid tank electroplating platinum and a synthetic method thereof, in particular structures of main salt-phosphoric acid tetrammineplatinum dihydrogen for novel acidic phosphoric acid tank plating platinum and main salt-phosphoric acid tetrammineplatinum for alkaline phosphoric acid tank plating platinum and synthetic methods thereof. The synthetic method comprises the following steps: chloride ions of tetrammineplatinum dichloride are precipitated by phosphoric acid dihydrogen silver to synthesize the phosphoric acid tetrammineplatinum dihydrogen; and chloride ions of the tetrammineplatinum dichloride are precipitated by silver phosphate to synthesize the phosphoric acid tetrammineplatinum. The synthetic method has the advantages of short flow, quick reaction speed, high yield (higher than 98.0%) and product purity higher than 99.0%, and is suitable for batch synthesis.

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