发明公开
- 专利标题: PROCEDE DE PRODUCTION DE PARAXYLENE COMPORTANT UNE CRISTALLISATION A HAUTE TEMPERATURE A AU MOINS UN ETAGE ET UNE FUSION PARTIELLE DES CRISTAUX
- 专利标题(英): Method for producing para-xylene by high-temperature crystallisation in at least one stage and partial crystal fusion
- 专利标题(中): 用于生产ON高温对二甲苯至少一个结晶步骤和晶体部分熔融含有STAGE
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申请号: EP96901408.0申请日: 1996-01-17
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公开(公告)号: EP0804394A1公开(公告)日: 1997-11-05
- 发明人: MacPHERSON, Stuart, R. , MIKITENKO, Paul
- 申请人: INSTITUT FRANCAIS DU PETROLE
- 申请人地址: 4, avenue de Bois Préau 92506 Rueil-Malmaison FR
- 专利权人: INSTITUT FRANCAIS DU PETROLE
- 当前专利权人: INSTITUT FRANCAIS DU PETROLE
- 当前专利权人地址: 4, avenue de Bois Préau 92506 Rueil-Malmaison FR
- 代理机构: Andreeff, François, et al
- 优先权: FR19950000746 19950120
- 国际公布: WO1996022262 19960725
- 主分类号: B01D9
- IPC分类号: B01D9 ; C07C6 ; C07C7 ; C07C15
摘要:
A method for producing para-xylene from a xylene-containing feedstock, wherein a first fraction is enriched to at least 30 wt.% with para-xylene, and said fraction is purified by means of at least one high-temperature crystallisation step performed in at least one crystallisation zone. Specifically, said first fraction enriched to at least 30 wt.% with para-xylene is crystallised in a crystallisation zone (50) at a high temperature (T1), advantageously between +10 and -25 °C, a suspension of crystals in a mother liquor is recovered, the crystals are separated from the mother liquor in at least a first separation zone (52), the resulting crystals are partially melted in at least one partial melting zone (55), a crystal suspension is recovered, the crystal suspension is separated and washed in at least one separation and washing zone (57), and pure para-xylene crystals and a washing liquor (58) are recovered, whereafter said pure crystals are optionally completely melted (61) and a liquid stream (60) of molten para-xylene is recovered. The mother liquor may be crystallised in a second crystallisation zone at a high temperature (T2) lower than the first (T1), and the second crystals may be partially melted, separated and washed as above.
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