发明公开
- 专利标题: VERFAHREN ZUR STEUERUNG DER KRISTALLGRÖSSE BEI DER KONTINUIERLICHEN MASSENKRISTALLISATION
- 专利标题(英): Method for controlling crystal size during continuous mass crystallisation
- 专利标题(中): 方法用于控制连续大规模结晶晶粒尺寸
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申请号: EP00916803.0申请日: 2000-03-09
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公开(公告)号: EP1165198A1公开(公告)日: 2002-01-02
- 发明人: SEIDEL, Birgit , ULLRICH, Peter , ZEIBIG, Michael , SCHMITT, Dieter
- 申请人: Domo Caproleuna GmbH
- 申请人地址: Am Haupttor 06237 Leuna DE
- 专利权人: Domo Caproleuna GmbH
- 当前专利权人: Domo Caproleuna GmbH
- 当前专利权人地址: Am Haupttor 06237 Leuna DE
- 代理机构: Schinke, Herbert, Dr. Dr., Patentanwaltskanzlei
- 优先权: DE19912699 19990320
- 国际公布: WO0056416 20000928
- 主分类号: B01D9/00
- IPC分类号: B01D9/00
摘要:
The invention relates to a method for controlling the crystal size during continuous mass crystallisation, especially with ammonium sulphate. According to said method, seed products are added, the seed product being produced independently of the current crystallisation process in terms of its parameters. The average grain size of the solid form of the seed product is 0.1 to 1.0 mm and is smaller than that of the desired crstallisate. The solid form of the seed product is produced from different technological sub-streams in the given grain size range, independently of the main crystallisation process. The temperature of the seed product when it is added is up to 40 °C, preferably 10 to 30 °C lower than the process temperature in the crystalliser and all other materials that are supplied or returned to the crystalliser are free of solids. By controlling the parameters of the seed product it is possible to influence the grain size distribution of the end product and significantly reduce the fluctuations in the distribution of the grain size of the end product. The method can be carried out with discontinuous or continuous addition of the seed product.
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