发明公开
EP1566398A1 Method for drying nonionic alkylene oxide-type water soluble resin, method for packaging it, and method for transporting it
审中-公开
用于干燥的烯化氧类型的非离子,水溶性树脂的方法,其用于包装和运输的方法
- 专利标题: Method for drying nonionic alkylene oxide-type water soluble resin, method for packaging it, and method for transporting it
- 专利标题(中): 用于干燥的烯化氧类型的非离子,水溶性树脂的方法,其用于包装和运输的方法
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申请号: EP05003336.4申请日: 2005-02-16
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公开(公告)号: EP1566398A1公开(公告)日: 2005-08-24
- 发明人: Kono, Michiyuki , Kikuta, Manabu , Tezuka, Masaki , Tanaka, Hiroshi , Yokohashi, Takao , Nishihata, Takao , Murata, Kazuhiko , Toba, Taketo , Tamura, Fumihide , Kitada, Ritsuo
- 申请人: DAI-ICHI KOGYO SEIYAKU CO., LTD. , NIPPON SHOKUBAI CO., LTD.
- 申请人地址: 55 Nishishichijo Higashikubo-cho Shimogyo-ku Kyoto JP
- 专利权人: DAI-ICHI KOGYO SEIYAKU CO., LTD.,NIPPON SHOKUBAI CO., LTD.
- 当前专利权人: DAI-ICHI KOGYO SEIYAKU CO., LTD.,NIPPON SHOKUBAI CO., LTD.
- 当前专利权人地址: 55 Nishishichijo Higashikubo-cho Shimogyo-ku Kyoto JP
- 代理机构: Strehl Schübel-Hopf & Partner
- 优先权: JP2004043470 20040219; JP2004043500 20040219; JP2004043518 20040219; JP2004046702 20040223
- 主分类号: C08G65/34
- IPC分类号: C08G65/34 ; C08G65/46 ; C08G65/02 ; C08G65/30
摘要:
For efficiently drying a nonionic alkylene oxide-type water-soluble resin to make it have a low water content within a short period of time, the resin is put into a container, then the container is degassed to a vacuum degree of at most 150 mmHg, and while the vacuum degree is kept as such, a dry gas having a dew point not higher than the dew point DP calculated according to the following formula (1) is introduced into the container at an introduction rate not lower than the introduction rate V calculated according to the following formula (2). For efficiently removing minor volatiles from a nonionic alkylene oxide-type water-soluble resin, used is a drying device that comprises an evaporation tank where the resin is put in and a stirring blade which revolves inside the evaporation tank as it rotates on its own axis. For protecting a dried nonionic alkylene oxide-type water-soluble resin from water, a preferred method comprises introducing a dry gas into a packing line that runs from a dry resin-feeding zone to a packaging container, thereby introducing the dry gas into the empty packaging container just before packed with the resin along with purging away the air initially existing in the container, then packing the packaging container with the resin, and sealing up the opening of the packaging container. A method of transporting a nonionic alkylene oxide-type water-soluble resin that ensures good processability of the resin and prevents the resin from being deteriorated comprises controlling the resin so as to have a solvent content of from 0.001 to 50 % by weight and a viscosity at 40°C of at most 10,000 Pa·sec, and loading it into a transportation container equipped with a temperature control capability and/or unloading it out of the transportation container by the use of a pump. DP (°C) = -21.6 log 10 Vac V (L/min) = 0.5 × [Vac/(273 + T)] × V 0 wherein Vac indicates the vacuum degree (mm Hg), T indicates the temperature inside the container (°C), V 0 indicates the volume of the container (ml).
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