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    Process for manufacturing a pellet-shaped nonionic alkylene oxide resin
    1.
    发明公开
    Process for manufacturing a pellet-shaped nonionic alkylene oxide resin 审中-公开
    Verfahren zur Herstellung pellet-förmigernichtionischer Alkylenoxide

    公开(公告)号：EP1728812A1

    公开(公告)日：2006-12-06

    申请号：EP06114779.9

    申请日：2006-05-31

    申请人： NIPPON SHOKUBAI CO., LTD. ,  DAI-ICHI KOGYO SEIYAKU CO., LTD.

    发明人： Tamura, Fumihide ,  Okada, Izuho ,  Wakami, Hideo ,  Toba, Taketo ,  Mizushima, Makoto ,  Takamiya, Shigetaka ,  Horo, Shinichi ,  Kono, Michiyuki ,  Tezuka, Masaki ,  Tanaka, Hiroshi ,  Yokohashi, Takao ,  Kikuta, Manabu

    IPC分类号： C08G65/26

    CPC分类号： C08J3/12 ,  C08G65/30 ,  C08J2371/02

    摘要： An object of the present invention is to provide a manufacturing process by which a pellet-shaped nonionic alkylene oxide resin can be obtained in a manner which is excellent in stability, economical efficiency and productivity and easy, wherein the pellet-shaped nonionic alkylene oxide resin, as a high-molecular material useful in a variety of applications, has a suitable molecular weight Mw and physical properties and is also excellent in the stability of the physical properties and further is also excellent in the handling property after the manufacture. As a means of achieving this object, the process for manufacturing a pellet-shaped nonionic alkylene oxide resin, according to the present invention, comprises the steps of: obtaining a nonionic alkylene oxide resin having fluidity by volatilizing a solvent from a nonionic alkylene oxide resin solution obtained in advance by solution polymerization; and then pelletizing the nonionic alkylene oxide resin having fluidity.

    摘要翻译： 本发明的目的是提供一种可以以稳定性，经济效率和生产率优异的方式获得丸状非离子环氧烷烃树脂的制备方法，其中颗粒状非离子环氧烷树脂 作为可用于各种应用的高分子材料，具有合适的分子量Mw和物理性质，并且在物理性能的稳定性方面也是优异的，并且还在制造后的处理性能也优异。 作为实现该目的的手段，根据本发明的颗粒状非离子性环氧烷烃树脂的制造方法包括以下步骤：通过从非离子性环氧烷树脂挥发溶剂获得具有流动性的非离子环氧烷烃树脂 溶液聚合预先得到的溶液; 然后造粒具有流动性的非离子环氧烷烃树脂。

    Method for drying nonionic alkylene oxide-type water soluble resin, method for packaging it, and method for transporting it
    2.
    发明公开
    Method for drying nonionic alkylene oxide-type water soluble resin, method for packaging it, and method for transporting it 审中-公开
    用于干燥的烯化氧类型的非离子，水溶性树脂的方法，其用于包装和运输的方法

    公开(公告)号：EP1566398A1

    公开(公告)日：2005-08-24

    申请号：EP05003336.4

    申请日：2005-02-16

    申请人： DAI-ICHI KOGYO SEIYAKU CO., LTD. ,  NIPPON SHOKUBAI CO., LTD.

    发明人： Kono, Michiyuki ,  Kikuta, Manabu ,  Tezuka, Masaki ,  Tanaka, Hiroshi ,  Yokohashi, Takao ,  Nishihata, Takao ,  Murata, Kazuhiko ,  Toba, Taketo ,  Tamura, Fumihide ,  Kitada, Ritsuo

    IPC分类号： C08G65/34 ,  C08G65/46 ,  C08G65/02 ,  C08G65/30

    CPC分类号： C08G65/30 ,  Y10T428/1348

    摘要： For efficiently drying a nonionic alkylene oxide-type water-soluble resin to make it have a low water content within a short period of time, the resin is put into a container, then the container is degassed to a vacuum degree of at most 150 mmHg, and while the vacuum degree is kept as such, a dry gas having a dew point not higher than the dew point DP calculated according to the following formula (1) is introduced into the container at an introduction rate not lower than the introduction rate V calculated according to the following formula (2). For efficiently removing minor volatiles from a nonionic alkylene oxide-type water-soluble resin, used is a drying device that comprises an evaporation tank where the resin is put in and a stirring blade which revolves inside the evaporation tank as it rotates on its own axis. For protecting a dried nonionic alkylene oxide-type water-soluble resin from water, a preferred method comprises introducing a dry gas into a packing line that runs from a dry resin-feeding zone to a packaging container, thereby introducing the dry gas into the empty packaging container just before packed with the resin along with purging away the air initially existing in the container, then packing the packaging container with the resin, and sealing up the opening of the packaging container. A method of transporting a nonionic alkylene oxide-type water-soluble resin that ensures good processability of the resin and prevents the resin from being deteriorated comprises controlling the resin so as to have a solvent content of from 0.001 to 50 % by weight and a viscosity at 40°C of at most 10,000 Pa·sec, and loading it into a transportation container equipped with a temperature control capability and/or unloading it out of the transportation container by the use of a pump. DP (°C) = -21.6 log 10 Vac V (L/min) = 0.5 × [Vac/(273 + T)] × V 0 wherein Vac indicates the vacuum degree (mm Hg), T indicates the temperature inside the container (°C), V 0 indicates the volume of the container (ml).

    摘要翻译： 为了有效地进行干燥的非离子烯属烃氧化物型水溶性树脂，使之具有很短的时间周期内的低水含量时，树脂放入容器中，然后将容器脱气至至多150毫米汞柱的真空度 ，并且在真空度保持为搜索，具有露点不大于计算雅丁以下公式露点DP高的干燥气体（1）在引入速率不大于导入速度V下引入容器 计算gemäß下面的公式（2）。 为有效地从非离子烯属烃氧化物型水溶性树脂，使用除去次要挥发物是干燥装置确实将树脂放入蒸发罐的包括和搅拌叶片在其旋转时在其自身的轴线的蒸发罐内哪个旋转 ， 用于保护干燥的非离子烯属烃氧化物类水溶性树脂选自水，优选的方法包括从干树脂进料区引入干燥气体进入包装线并延伸到包装容器中，从而引入干燥气体送入空 包装容器刚刚填充了树脂非常久远吹扫出空气初始存在于容器中，然后用树脂填充的包装容器，和密封起来包装容器的开口部之前。 确实输送非离子烯属烃氧化物型水溶性树脂的方法，确保了树脂的良好加工性和的恶化包括控制树脂，以便通过重量和粘度以具有从0.001％至50％的溶剂含量防止树脂 在40℃下至多万帕·秒，并且加载到配备有温度控制能力和/或通过使用泵的卸出来的运输容器的运输容器。 DP（℃）= -21.6日志10伏交流 V（升/分钟）= 0.5×AVAC /（273 + T）ÜX V0 worin吸尘器指示真空度（毫米汞柱），T表示所述容器（℃）内部的温度，V0表示所述容器（毫升）的体积。