发明公开
EP2128122A1 PROCESS FOR PRODUCING CARBOXYLIC ACID CHLORIDE
有权
VERFAHREN ZUR HERSTELLUNG EINESCARBONSÄURECHLORIDS
- 专利标题: PROCESS FOR PRODUCING CARBOXYLIC ACID CHLORIDE
- 专利标题(中): VERFAHREN ZUR HERSTELLUNG EINESCARBONSÄURECHLORIDS
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申请号: EP08712044.0申请日: 2008-02-27
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公开(公告)号: EP2128122A1公开(公告)日: 2009-12-02
- 发明人: KOBAYASHI, Takeshi , KIDO, Kiyomi , NAGATOMO, Akinori
- 申请人: Mitsui Chemicals, Inc.
- 申请人地址: 5-2, Higashi-Shimbashi 1-chome Minato-ku Tokyo 105-7117 JP
- 专利权人: Mitsui Chemicals, Inc.
- 当前专利权人: Mitsui Chemicals, Inc.
- 当前专利权人地址: 5-2, Higashi-Shimbashi 1-chome Minato-ku Tokyo 105-7117 JP
- 代理机构: Stuart, Ian Alexander
- 优先权: JP2007051879 20070301
- 国际公布: WO2008105464 20080904
- 主分类号: C07C51/60
- IPC分类号: C07C51/60 ; C07C51/64 ; C07C55/36
摘要:
This invention relates to a method for producing a carboxylic acid chloride, which efficiently decomposes a Vilsmeier reagent type compound in a carboxylic acid chloride lacking a thermal stability or a carboxylic acid chloride hardly distilled in practice due to a high boiling point with a simple operation and has no adverse effect on a subsequent step, and more particularly to a method for producing a carboxylic acid chloride, characterized by comprising reacting a carboxylic acid with a chlorinating agent in the presence of a catalyst, removing the excessive chlorinating agent from a reaction system after the reaction, and then further adding 1.0 to 3.0 equivalents of the starting carboxylic acid based on the catalyst to the reaction system to decompose a Vilsmeier reagent type compound remaining in the reaction system.
公开/授权文献
- EP2128122B1 PROCESS FOR PRODUCING CARBOXYLIC ACID CHLORIDE 公开/授权日:2014-01-22
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