发明公开
EP2708511A4 METHOD FOR MANUFACTURING TIN(II) OXIDE POWDER FOR REPLENISHING TIN COMPONENT OF TIN-ALLOY PLATING SOLUTION, AND TIN(II) OXIDE POWDER MANUFACTURED USING SAID METHOD
审中-公开
用于生产氧化亚锡粉末用于补充电镀的锡组分FOR锡合金,在这种方法制得的氧化亚锡粉末
- 专利标题: METHOD FOR MANUFACTURING TIN(II) OXIDE POWDER FOR REPLENISHING TIN COMPONENT OF TIN-ALLOY PLATING SOLUTION, AND TIN(II) OXIDE POWDER MANUFACTURED USING SAID METHOD
- 专利标题(中): 用于生产氧化亚锡粉末用于补充电镀的锡组分FOR锡合金,在这种方法制得的氧化亚锡粉末
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申请号: EP12781588申请日: 2012-05-08
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公开(公告)号: EP2708511A4公开(公告)日: 2014-10-29
- 发明人: KATASE TAKUMA , MASUDA AKIHIRO , KUBA KANJI
- 申请人: MITSUBISHI MATERIALS CORP
- 专利权人: MITSUBISHI MATERIALS CORP
- 当前专利权人: MITSUBISHI MATERIALS CORP
- 优先权: JP2011104952 2011-05-10
- 主分类号: C01G19/02
- IPC分类号: C01G19/02 ; C25D3/60 ; C25D21/14
摘要:
An object and a problem of the present invention is to provide tin(II) oxide powder which has extremely high solubility in an acid or an acidic plating solution, excellent in storage stability in the air and can heighten oxidation-preventive effect of Sn 2+ ion in the plating solution. The method for manufacturing tin(II) oxide powder of the present invention comprises Step (11) of preparing an aqueous acidic solution containing Sn 2+ ions, Step (12) of neutralizing the aqueous acidic solution by adding an aqueous alkaline solution to prepare a slurry of tin(II) hydroxide, Step (13) of dehydrating the prepared slurry to obtain a slurry of tin(II) oxide, Step (14) of separating the slurry of tin(II) oxide into a solid and a liquid to obtain tin(II) oxide, Step (15) of treating the obtained tin(II) oxide with an aqueous antioxidant solution, and Step (16) of vacuum drying the tin(II) oxide treated with the aqueous antioxidant solution. Also, the tin(II) oxide powder of the present invention is suitable for replenishing a tin component to a tin-alloy plating solution.
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