发明专利
- 专利标题: Method for producing n,n-dialkylhomofarnesic acid amide
- 专利标题(中): 生产N,N-二烷基戊酸酰胺的方法
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申请号: JP2013209087申请日: 2013-10-04
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公开(公告)号: JP2014097970A公开(公告)日: 2014-05-29
- 发明人: YANO KENJI , AOKI TAKASHI
- 申请人: Kao Corp , 花王株式会社
- 专利权人: Kao Corp,花王株式会社
- 当前专利权人: Kao Corp,花王株式会社
- 优先权: JP2012232075 2012-10-19
- 主分类号: C07C231/10
- IPC分类号: C07C231/10 ; C07C233/09 ; C07D307/92
摘要:
PROBLEM TO BE SOLVED: To provide a method for producing an N,N-dialkylhomofarnesic acid amide which is a precursor of (±)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan useful as a fragrance with a high raw material recovery rate, high purity and high yield and a method for producing (±)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan.SOLUTION: There is provided a method for producing an N,N-dialkylhomofarnesic acid amide by reacting nerolidol with N,N-dialkylformamide dimethyl acetal under conditions where the N,N-dialkylformamide dimethyl acetal is refluxed, wherein the molar ratio of the N,N-dialkylformamide dimethyl acetal to nerolidol is 1.5 to 3.
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