Invention Grant
- Patent Title: Process for the preparation of a purified acid composition
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Application No.: US15579257Application Date: 2016-06-06
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Publication No.: US10351544B2Publication Date: 2019-07-16
- Inventor: Ana Rita Martins Guerreiro Rocha Almeida , Martinus Mathilda Pieter Zieverink , Ana Sofia Vagueiro De Sousa Dias
- Applicant: Synvina C.V.
- Applicant Address: NL Amsterdam
- Assignee: Synvina C.V.
- Current Assignee: Synvina C.V.
- Current Assignee Address: NL Amsterdam
- Agency: Hoffmann & Baron, LLP
- Priority: NL2014923 20150605
- International Application: PCT/NL2016/050404 WO 20160606
- International Announcement: WO2016/195499 WO 20161208
- Main IPC: B01J23/34
- IPC: B01J23/34 ; B01J23/75 ; B01J27/08 ; C07B31/00 ; C07B33/00 ; C07B41/02 ; C07B63/02 ; C07D307/68

Abstract:
A purified acid composition including 2,5-furandicarboxylic acid is prepared by a process including a) providing an acid composition solution of a crude acid composition in a polar solvent, the crude acid composition including 2,5-furandicarboxylic acid (FDCA) and 2-formyl-furan-5-carboxylic acid (FFCA); b) contacting the acid composition solution with hydrogen in the presence of a hydrogenation catalyst to hydrogenate FFCA to hydrogenation products, such that the hydrogenation products contain a minor amount of 2-methyl-furan-5-carboxylic acid (MFA) or no MFA, yielding a hydrogenated solution; c) separating at least a portion of the FDCA from the hydrogenated solution by crystallization.
Public/Granted literature
- US20180155309A1 PROCESS FOR THE PREPARATION OF A PURIFIED ACID COMPOSITION Public/Granted day:2018-06-07
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