Invention Grant
- Patent Title: Process for purification of methyl methacrylate
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Application No.: US15768027Application Date: 2016-09-28
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Publication No.: US10392337B2Publication Date: 2019-08-27
- Inventor: Dennis W. Jewell , John G. Pendergast, Jr. , William G. Worley
- Applicant: Dow Global Technologies LLC
- Applicant Address: US MI Midland
- Assignee: Dow Global Technologies LLC
- Current Assignee: Dow Global Technologies LLC
- Current Assignee Address: US MI Midland
- Agent Brian L. Mutschler
- International Application: PCT/US2016/054043 WO 20160928
- International Announcement: WO2017/065969 WO 20170420
- Main IPC: B01D3/06
- IPC: B01D3/06 ; B01D3/14 ; C07C51/44 ; C07C57/04 ; C07C67/54 ; C07C69/54 ; B01L3/14 ; B01L3/06

Abstract:
A process for purifying methyl methacrylate. The method comprises: (a) feeding a product mixture comprising methyl methacrylate, methanol, water and oligomers of methyl methacrylate to a divided section of a distillation column comprising a dividing wall; (b) removing an overhead stream and a bottoms stream from the distillation column, and removing a middle side draw stream from the distillation column; wherein the crude product enters the dividing wall distillation column in a divided section on an opposing side of the dividing wall from the middle side draw stream; and (c) removing an upper side draw stream from a point above the dividing wall and below the top of the distillation column, separating a portion of water from the upper side draw stream to produce a dewatered upper side draw stream and returning the dewatered upper side draw stream to the distillation column.
Public/Granted literature
- US20180297930A1 PROCESS FOR PURIFICATION OF METHYL METHACRYLATE Public/Granted day:2018-10-18
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