Invention Grant
- Patent Title: Method for preparing pressed scandia-doped dispenser cathodes using microwave sintering
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Application No.: US15409888Application Date: 2017-01-19
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Publication No.: US10651000B2Publication Date: 2020-05-12
- Inventor: Wei Liu , Mingchaung Tian , Jinshu Wang , Fan Zhou , Yiman Wang , Liran Dong , Yunfei Yang , Quan Zhang
- Applicant: Beijing University of Technology
- Applicant Address: CN Beijing
- Assignee: Beijing University of Technology
- Current Assignee: Beijing University of Technology
- Current Assignee Address: CN Beijing
- Agent Zhihua Han
- Priority: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@241fa488
- Main IPC: B22F3/105
- IPC: B22F3/105 ; H01J9/04 ; B22F9/02 ; B22F9/22 ; C22B34/36 ; B22F9/30 ; H01J1/28 ; H01J19/22 ; H01J35/06

Abstract:
The present disclosure discloses a preparation method of pressed Scandia-doped dispenser cathode using microwave sintering. Embodiments of the present disclosure include dissolving some nitrates and ammonium metatungstate with deionized water to prepare a homogeneous solution. Precursor powder with uniform size is obtained by spray drying, the precursor powder is decomposed, and two-step reduction may be proceeded to form doped tungsten powder with uniform element distribution. The cathode is prepared by one-time microwave sintering. One-time forming of cathode sintering is realized, and sintering shrinkage and sintering time are reduced significantly. The method has excellent repeatability, and the cathode has a homogeneous structure and excellent emission performance at 950° C.
Public/Granted literature
- US20170345608A1 Method for preparing pressed scandia-doped dispenser cathodes using microwave sintering Public/Granted day:2017-11-30
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