Invention Grant
- Patent Title: Process for preparing an epoxidation catalyst
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Application No.: US16328033Application Date: 2017-08-30
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Publication No.: US10821430B2Publication Date: 2020-11-03
- Inventor: Mohmed A. Syed , Apoorva Kulkarni , Vera P. Santos Castro , Victor J. Sussman , John C. McKeen , Cathy L. Tway , Clifford S. Todd
- Applicant: Dow Technology Investments LLC
- Applicant Address: US MI Midland
- Assignee: Dow Technology Investments LLC
- Current Assignee: Dow Technology Investments LLC
- Current Assignee Address: US MI Midland
- International Application: PCT/US2017/049287 WO 20170830
- International Announcement: WO2018/044982 WO 20180308
- Main IPC: B01J37/02
- IPC: B01J37/02 ; B01J23/50 ; B01J37/00 ; C07C213/04 ; C07D301/10 ; C07D317/36 ; C07C215/08 ; C07D317/04 ; B01J21/04 ; B01J35/10 ; B01J37/08 ; C07C29/00 ; C07C41/02 ; C07C68/00 ; C07C213/00 ; C07D301/03

Abstract:
A process for preparing a silver-containing catalyst for the selective oxidation of ethylene to ethylene oxide including the steps of: (a) providing a multimodal support, (b) preparing an impregnation solution comprising a silver component, (c) impregnating, at least once, the multimodal support of step (a) with the silver-containing impregnation solution of step (b) to form an impregnated support; (d) subjecting the impregnated multimodal support from step (c) to a removal means, such as a centrifuge, at least once, for a time sufficient to remove impregnated silver impregnation solution from the multimodal support and to control the amount of silver in the pores of the multimodal support by selectively removing impregnated silver impregnation solution from a set of larger pores in the multimodal support; (e) roasting, at least once, the multimodal support after the step (d); (f) optionally, repeating the impregnation step (c), (g) optionally, repeating the centrifugation step (d), and (h) optionally, repeating the calcination step (e).
Public/Granted literature
- US20190184387A1 PROCESS FOR PREPARING AN EPOXIDATION CATALYST Public/Granted day:2019-06-20
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