Invention Grant
- Patent Title: Thin-sheet zeolite membrane and methods for making the same
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Application No.: US16272885Application Date: 2019-02-11
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Publication No.: US10953372B2Publication Date: 2021-03-23
- Inventor: Wei Liu
- Applicant: Battelle Memorial Institute
- Applicant Address: US WA Richland
- Assignee: Battelle Memorial Institute
- Current Assignee: Battelle Memorial Institute
- Current Assignee Address: US WA Richland
- Agency: Klarquist Sparkman, LLP
- Main IPC: B01D71/02
- IPC: B01D71/02 ; B01D69/10 ; B01D67/00 ; B01D39/20 ; B01D69/06 ; B22F5/00 ; C22C19/00 ; C22C19/03 ; C22C38/08 ; C22C28/00

Abstract:
Zeolite membrane sheets for separation of mixtures containing water are provided, as well as methods for making the same. Thin, but robust, zeolite membrane sheets having an inter-grown zeolite crystal film directly on a thin, less than 200 micron thick, porous support sheet free of any surface pores with a size above 10 microns. The zeolite membrane film thickness is less than about 10 microns above the support surface and less than about 5 microns below the support surface. Methods of preparing the membrane are disclosed which include coating of the support sheet surface with a seed coating solution containing the parent zeolite crystals with mean particle sizes from about 0.5 to 2.0 microns at loading of 0.05-0.5 mg/cm2 and subsequent growth of the seeded sheet in a growth reactor loaded with a growth solution over a temperature range of about 45° C. to about 120° C.
Public/Granted literature
- US20190176097A1 THIN-SHEET ZEOLITE MEMBRANE AND METHODS FOR MAKING THE SAME Public/Granted day:2019-06-13
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