Invention Grant
- Patent Title: Method for controlled preparation of low molecular weight cellulose ether
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Application No.: US16608892Application Date: 2018-06-29
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Publication No.: US11407842B2Publication Date: 2022-08-09
- Inventor: Robert B. Appell , Joseph L Weir
- Applicant: DOW GLOBAL TECHNOLOGIES LLC
- Applicant Address: US MI Midland
- Assignee: DOW GLOBAL TECHNOLOGIES LLC
- Current Assignee: DOW GLOBAL TECHNOLOGIES LLC
- Current Assignee Address: US MI Midland
- International Application: PCT/US2018/040196 WO 20180629
- International Announcement: WO2019/036123 WO 20190221
- Main IPC: C08B11/08
- IPC: C08B11/08

Abstract:
A process includes: (a) providing an initial cellulose ether powder containing 0.5 to 10 weight-percent water based on total cellulose ether powder weight; (b) heating the initial cellulose ether powder to a temperature in a range of 30 to 130 degrees Celsius; (c) before, during and/or after heating in step (b), adding solid base to the cellulose ether powder and mixing with the initial cellulose ether powder to form a cellulose ether/base mixture; (d) adding volatile acid to the cellulose ether/base mixture and mixing; and (e) allowing the volatile acid to hydrolyze the initial cellulose ether to form a final cellulose ether having a lower viscosity than the initial cellulose ether.
Public/Granted literature
- US20200181290A1 METHOD FOR CONTROLLED PREPARATION OF LOW MOLECULAR WEIGHT CELLULOSE ETHER Public/Granted day:2020-06-11
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