• Patent Title: Impact of trace elements in the Grignard reaction
  • Application No.: US17442862
    Application Date: 2020-03-25
  • Publication No.: US11697641B2
    Publication Date: 2023-07-11
  • Inventor: Joerg BaeuchleWolfgang Wiesenhoefer
  • Applicant: BASF SE
  • Applicant Address: DE Ludwigshafen am Rhein
  • Assignee: BASF SE
  • Current Assignee: BASF SE
  • Current Assignee Address: DE Ludwigshafen am Rhein
  • Agency: Faegre Drinker Biddle & Reath LLP
  • Priority: EP 165605 2019.03.27
  • International Application: PCT/EP2020/058327 2020.03.25
  • International Announcement: WO2020/193617A 2020.10.01
  • Date entered country: 2021-09-24
  • Main IPC: C07D251/20
  • IPC: C07D251/20
Impact of trace elements in the Grignard reaction
Abstract:
The present invention relates to an improved process for preparing 2,4-dichloro-6-(4-methoxyphenyl)-1,3,5-triazine (DICAT) comprising reacting 4-bromoanisole with magnesium, and reacting the resulting Grignard reagent with cyanuric chloride, wherein the magnesium comprises additional metals as impurities in an amount of less than 0.027% by weight, based on the total weight of the magnesium.
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