Invention Grant
- Patent Title: Impact of trace elements in the Grignard reaction
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Application No.: US17442862Application Date: 2020-03-25
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Publication No.: US11697641B2Publication Date: 2023-07-11
- Inventor: Joerg Baeuchle , Wolfgang Wiesenhoefer
- Applicant: BASF SE
- Applicant Address: DE Ludwigshafen am Rhein
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen am Rhein
- Agency: Faegre Drinker Biddle & Reath LLP
- Priority: EP 165605 2019.03.27
- International Application: PCT/EP2020/058327 2020.03.25
- International Announcement: WO2020/193617A 2020.10.01
- Date entered country: 2021-09-24
- Main IPC: C07D251/20
- IPC: C07D251/20

Abstract:
The present invention relates to an improved process for preparing 2,4-dichloro-6-(4-methoxyphenyl)-1,3,5-triazine (DICAT) comprising reacting 4-bromoanisole with magnesium, and reacting the resulting Grignard reagent with cyanuric chloride, wherein the magnesium comprises additional metals as impurities in an amount of less than 0.027% by weight, based on the total weight of the magnesium.
Public/Granted literature
- US20220251050A1 IMPACT OF TRACE ELEMENTS IN THE GRIGNARD REACTION Public/Granted day:2022-08-11
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