Impact of trace elements in the Grignard reaction

    公开(公告)号:US11697641B2

    公开(公告)日:2023-07-11

    申请号:US17442862

    申请日:2020-03-25

    Applicant: BASF SE

    CPC classification number: C07D251/20

    Abstract: The present invention relates to an improved process for preparing 2,4-dichloro-6-(4-methoxyphenyl)-1,3,5-triazine (DICAT) comprising reacting 4-bromoanisole with magnesium, and reacting the resulting Grignard reagent with cyanuric chloride, wherein the magnesium comprises additional metals as impurities in an amount of less than 0.027% by weight, based on the total weight of the magnesium.

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