- Patent Title: Method and apparatus for preparing transition metal lithium oxide
-
Application No.: US16609742Application Date: 2019-05-31
-
Publication No.: US11757095B2Publication Date: 2023-09-12
- Inventor: Huibin Zhang , Ying Wang , Jinfu Wang , Hongdong Zhao , Longwei Niu
- Applicant: SHANDONG ZSTONE NEW MATERIAL TECHNOLOGY CO., LTD.
- Applicant Address: CN Shandong
- Assignee: SHANDONG ZSTONE NEW MATERIAL TECHNOLOGY CO., LTD.
- Current Assignee: SHANDONG ZSTONE NEW MATERIAL TECHNOLOGY CO., LTD.
- Current Assignee Address: CN Shandong
- Agent Yue (Robert) Xu
- Priority: CN 1910371372.8 2019.05.06 CN 1920637155.4 2019.05.06 CN 1910433634.9 2019.05.23
- International Application: PCT/CN2019/089422 2019.05.31
- International Announcement: WO2020/224020A 2020.11.12
- Date entered country: 2019-10-31
- Main IPC: H01B1/08
- IPC: H01B1/08 ; H01M4/525 ; B01J8/00 ; B01J8/08 ; B01J8/12 ; C01G53/00 ; H01M4/505 ; H01M4/04

Abstract:
The present disclosure provides a method for preparing a transition metal lithium oxide, comprising steps of: A) mixing a lithium salt and a transition metal compound, and performing a pretreatment to obtain a precursor; wherein the pretreatment temperature is 100-300° C.; and the pretreatment time is 1-10 h; B) precalcining the precursor to obtain an intermediate; and C) continuously feeding the intermediate into a feed port of a moving bed reactor, and calcining, to obtain a transition metal lithium oxide. In the present disclosure, a pretreatment process is performed before the precalcination, and the pretreatment temperature and time are further limited, thereby solving the problem of material hardening during the calcination process of battery materials. In conjunction with using a moving bed reactor, the gas phase and the solid phase are sufficiently contacted, and at the same time the thickness of the filler is increased, the productivity is enhanced and the oxygen consumption is largely decreased at the same time. The present disclosure further provides an apparatus for preparing a transition metal lithium oxide.
Public/Granted literature
- US20210336261A1 METHOD AND APPARATUS FOR PREPARING TRANSITION METAL LITHIUM OXIDE Public/Granted day:2021-10-28
Information query