发明申请
- 专利标题: Method for producing barium titanate based powders by oxalate process
- 专利标题(中): 通过草酸盐法生产钛酸钡基粉末的方法
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申请号: US09871286申请日: 2001-05-31
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公开(公告)号: US20020048547A1公开(公告)日: 2002-04-25
- 发明人: Jai Joon Lee , Kang Heon Hur
- 申请人: Samsung Electro-Mechanics Co., Ltd.
- 申请人地址: null
- 专利权人: Samsung Electro-Mechanics Co., Ltd.
- 当前专利权人: Samsung Electro-Mechanics Co., Ltd.
- 当前专利权人地址: null
- 优先权: KR2000-46125 20000809
- 主分类号: C01G023/04
- IPC分类号: C01G023/04
摘要:
The present invention discloses a method for preparing a barium titanate and barium titanate based powder by an oxalate process. The method is carried out in the following manner: An aqueous mixture solution containing barium chloride and titanium chloride is added into an aqueous oxalic acid solution, so that barium titanyl oxalate would be precipitated. Then the precipitates are aged, washed and filtered. The filtered barium titanyl oxalate precipitates are crushed, and dried. Then a thermal decomposition is carried out to obtain a agglomerated barium titanate powder, and this is crushed again to obtain the final barium titanate powder. In order to obtain barium titanate based powder such as Ba(Ti1nullzZrz)O3, (Ba1nullxCax)(Ti1nullzZrz)O3, and (Ba1nullxnullyCaxSry)(Ti1nullzZrz)O3, the desired elements (Ca, Sr, Zr and so on) are added to barium titanyl oxalate when crushed before thermal decomposition step. After thermal decomposition and crushing, the barium titanate based powder can be obtained.