发明申请
US20040050251A1 Method and device for vaporization injection of high volumes in gas chromatographic analysis 有权
在气相色谱分析中大量气化注入的方法和装置

  • 专利标题: Method and device for vaporization injection of high volumes in gas chromatographic analysis
  • 专利标题(中): 在气相色谱分析中大量气化注入的方法和装置
  • 申请号: US10450165
    申请日: 2003-07-30
  • 公开(公告)号: US20040050251A1
    公开(公告)日: 2004-03-18
  • 发明人: Paolo Magni
  • 优先权: ITMI2001A002840 20011228
  • 主分类号: B01D053/02
  • IPC分类号: B01D053/02
Method and device for vaporization injection of high volumes in gas chromatographic analysis
摘要:
This invention concerns a method and apparatus for vaporization injection of large volumes of liquid sample (substance to be analysednullsolvent) introduced by means of the needle of a syringe onto a heated vaporization chamber which is part of an injector applied to a device for gas chromatographic analysis, the sample being sent in form of a liquid band travelling through said vaporization chamber at high speed until reaching stopping and vaporization means positioned adjacent to the inlet of a capillary to collect the vapours. In order to inject large volumes without modifying the vaporization chamber and without samples parts losses, in splitless mode, a drawing up of the sample vapours from the vaporization chamber into said capillary is made by means of a local action of volume contraction, caused by recondensation of at least the solvent vapours in this capillary, said capillary being in the form of a pre-column with no stationary phase, maintained at low temperature at least during the injection.
信息查询
0/0