发明申请
- 专利标题: NMR spectrometer with refrigerator cooling
- 专利标题(中): NMR光谱仪带冰箱冷却
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申请号: US11236555申请日: 2005-09-28
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公开(公告)号: US20060096301A1公开(公告)日: 2006-05-11
- 发明人: Rene Triebe , Daniel Marek , Oskar Schett , Daniel Baumann
- 申请人: Rene Triebe , Daniel Marek , Oskar Schett , Daniel Baumann
- 申请人地址: CH Faellanden
- 专利权人: Bruker BioSpin AG
- 当前专利权人: Bruker BioSpin AG
- 当前专利权人地址: CH Faellanden
- 优先权: DE102004053973.1 20041109
- 主分类号: F25B9/00
- IPC分类号: F25B9/00 ; F25B19/00 ; F25D23/12
摘要:
An NMR spectrometer comprising an NMR magnet system (27) disposed in a helium tank of a cryostat and an NMR probe head (11) disposed in a room temperature bore of the cryostat, which contains a cooled RF resonator (9) for receiving NMR signals from a sample to be investigated, and a cooled pre-amplifier (10), wherein the NMR probe head (11) is cooled by a common multi-stage compressor-operated refrigerator (2), wherein the refrigerator (2) comprises a cold head and several heat exchangers (5, 6) at different temperature levels, wherein the refrigerator (2) is disposed at a spatial separation from the cryostat in a separate, evacuated and thermally insulated housing (1) and wherein at least one cooling circuit with cooling lines, which are thermally insulated by a transfer line (13, 14) is disposed between the housing (1) containing the heat exchangers (5, 6) and the NMR probe head (11), is characterized in that additional cooling lines to an LN2 tank (18) or radiation shield (21) disposed in the cryostat and surrounding the helium tank are provided, and the refrigerator (2) also cools the LN2 tank (18) or the radiation shield (21). The inventive NMR spectrometer comprises a simple and inexpensive device for matching the holding time of LN2 to that of LHe through cooling the LN2 tank using the refrigerator provided for cooling the NMR probe head and without great expense.
公开/授权文献
- US07222490B2 NMR spectrometer with refrigerator cooling 公开/授权日:2007-05-29
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