发明申请
US20090062565A1 Continuous Process for the Production of mono- or dicarboxylic acid alkyl amides
有权
用于生产单羧酸或二羧酸烷基酰胺的连续方法
- 专利标题: Continuous Process for the Production of mono- or dicarboxylic acid alkyl amides
- 专利标题(中): 用于生产单羧酸或二羧酸烷基酰胺的连续方法
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申请号: US12293509申请日: 2007-03-09
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公开(公告)号: US20090062565A1公开(公告)日: 2009-03-05
- 发明人: Joaquin Bigorra Llosas , Javier Raya , Emilio Brau Balague , Manuel Seva , Ivan Francia , Ramon Valls
- 申请人: Joaquin Bigorra Llosas , Javier Raya , Emilio Brau Balague , Manuel Seva , Ivan Francia , Ramon Valls
- 申请人地址: DE Duesseldorf
- 专利权人: Cognis IP Management GmbH
- 当前专利权人: Cognis IP Management GmbH
- 当前专利权人地址: DE Duesseldorf
- 优先权: EPEP06005589 20060318
- 国际申请: PCT/EP2007/002072 WO 20070309
- 主分类号: C07C231/02
- IPC分类号: C07C231/02
摘要:
A continuous process for the production of mono- or dicarboxylic acid alkyl amides is described, which is characterized in that: fresh mono- or dicarboxylic acid is placed into a first reactor (R1) connected with a distillation column (C1) and subjected to a reaction with ammonia or gaseous alkyl amine to form a pre-mixture consisting of mono- or dicarboxylic acid alkyl amide and unreacted mono- or dicarboxylic acid, while the water of condensation is distilled off; said pre-mixture is transferred into a second reactor (R2) also equipped with a distillation column (C2) and subjected to a further reaction with ammonia or gaseous alkyl amine to substantially convert all unreacted mono- or dicarboxylic acid into mono- or dicarboxylic acid alkyl amide; and all unreacted ammonia or gaseous alkyl amine is transferred into the first reactor (R1) to start the amidation reaction.
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