发明申请
US20090259068A1 REACTION SYSTEMS FOR MAKING N-(PHOSPHONOMETHYL) GLYCINE COMPOUNDS
审中-公开
制备N-(膦酰基)乙酰化合物的反应体系
- 专利标题: REACTION SYSTEMS FOR MAKING N-(PHOSPHONOMETHYL) GLYCINE COMPOUNDS
- 专利标题(中): 制备N-(膦酰基)乙酰化合物的反应体系
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申请号: US12365507申请日: 2009-02-04
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公开(公告)号: US20090259068A1公开(公告)日: 2009-10-15
- 发明人: Eric Haupfear , Jerald D. Heise , Amy L. Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark A. Leiber , Kent Wittler , Karen A. Wittler
- 申请人: Eric Haupfear , Jerald D. Heise , Amy L. Jorgenson , Michael Rogers , Henry Chien , Eduardo Casanova , William Hooper , William Scholle , Juan Arhancet , Mark A. Leiber , Kent Wittler , Karen A. Wittler
- 申请人地址: US MO St. Louis
- 专利权人: MONSANTO TECHNOLOGY LLC
- 当前专利权人: MONSANTO TECHNOLOGY LLC
- 当前专利权人地址: US MO St. Louis
- 主分类号: C07F9/38
- IPC分类号: C07F9/38 ; B01D1/00 ; B01D9/00
摘要:
This invention generally relates to liquid phase oxidation processes for making N-(phosphonomethyl)glycine (also known in the agricultural chemical industry as glyphosate) and related compounds. This invention, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid (NPMIDA) substrate (i.e., N-(phosphonomethyl)iminodiacetic acid, a salt of N-(phosphonomethyl)iminodiacetic acid, or an ester of N-(phosphonomethyl)iminodiacetic acid) is continuously oxidized to form an N-(phosphonomethyl)glycine product (i.e., N-(phosphonomethyl)glycine, a salt of N-(phosphonomethyl)glycine, or an ester of N-(phosphonomethyl)glycine). This invention also, for example, particularly relates to processes wherein an N-(phosphonomethyl)iminodiacetic acid substrate is oxidized to form an N-(phosphonomethyl)glycine product, which, in turn, is crystallized (at least in part) in an adiabatic crystallizer.
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