发明申请
- 专利标题: POLYESTER RESIN PARTICLE AND METHOD FOR PRODUCING THE SAME
- 专利标题(中): 聚酯树脂颗粒及其生产方法
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申请号: US12301725申请日: 2007-08-02
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公开(公告)号: US20090263661A1公开(公告)日: 2009-10-22
- 发明人: Michiko Yoshida , Takeyuki Doi , Naoya Maeda , Hisashi Kimura
- 申请人: Michiko Yoshida , Takeyuki Doi , Naoya Maeda , Hisashi Kimura
- 申请人地址: JP Minato-ku
- 专利权人: Mitsubishi Chemical Corporation
- 当前专利权人: Mitsubishi Chemical Corporation
- 当前专利权人地址: JP Minato-ku
- 优先权: JP2006-211120 20060802; JP2007-045772 20070226
- 国际申请: PCT/JP07/65190 WO 20070802
- 主分类号: B32B27/36
- IPC分类号: B32B27/36 ; C08G63/78
摘要:
Polyester resin particles are provided as those capable of providing a highly transparent molded product by thermoforming, while suppressing fusion of the polyester prepolymer particles in a heat treatment thereof such as crystallization or solid-phase polycondensation, without reduction in a solid-phase polycondensation rate.The present invention provides a method for producing a polyester resin, comprising carrying out a hot-water treatment and a heat treatment, in this order, of polyester prepolymer particles obtained by melt polycondensation of a dicarboxylic acid component and a diol component. The hot-water treatment comprises bringing the polyester prepolymer particles with an intrinsic viscosity of from at least 0.10 dL/g to at most 1.0 dL/g and with a density of at most 1.36 g/cm3 into contact with hot water at a temperature higher than the glass transition temperature of the polyester prepolymer particles and less than 100° C., under the condition satisfying the following formula (1): 40≦(T−Tg)t≦6000 (1) wherein t is a hot-water treatment time (second), T is the temperature of the hot water (° C.) and Tg is the glass transition temperature (° C.) of the polyester prepolymer particles.
公开/授权文献
- US08329857B2 Polyester resin particle and method for producing the same 公开/授权日:2012-12-11
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