发明申请
US20110083957A1 Continuous Method For Producing Amides Of Aliphatic Hydroxycarboxylic Acids
审中-公开
连续生产脂肪族羟基羧酸酰胺的方法
- 专利标题: Continuous Method For Producing Amides Of Aliphatic Hydroxycarboxylic Acids
- 专利标题(中): 连续生产脂肪族羟基羧酸酰胺的方法
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申请号: US12935308申请日: 2009-03-18
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公开(公告)号: US20110083957A1公开(公告)日: 2011-04-14
- 发明人: Matthias Krull , Roman Morschhaeuser , Joachim Hess , Robert Milbradt , Franz-Xaver Scherl , Andreas Wacker , Michael Seebach , Joerg Appel
- 申请人: Matthias Krull , Roman Morschhaeuser , Joachim Hess , Robert Milbradt , Franz-Xaver Scherl , Andreas Wacker , Michael Seebach , Joerg Appel
- 申请人地址: VG Tortola
- 专利权人: CLARIANT FINANCE (BVI) LIMITED
- 当前专利权人: CLARIANT FINANCE (BVI) LIMITED
- 当前专利权人地址: VG Tortola
- 优先权: DE102008017213.8 20080404
- 国际申请: PCT/EP09/01989 WO 20090318
- 主分类号: B01J19/12
- IPC分类号: B01J19/12
摘要:
The invention relates to a continuous method for producing hydroxycarboxylic acid amides, according to which at least one hydroxycarboxylic acid of formula (I) HO—R3—COOH (I) wherein R3 is an optionally substituted aliphatic hydrocarbon group comprising between 1 and 100 carbon atoms, is reacted with at least one amine of formula (II) HNR1R2 (II) wherein R1 and R2 are independently hydrogen or a carbon group comprising between 1 and 100 C atoms, to form an ammonium salt, and said ammonium salt is then reacted to form a hydroxycarboxylic acid amide, under microwave irradiation in a reaction pipe, the longitudinal axis of the pipe being oriented in the direction of propagation of the microwaves of a monomode microwave applicator.
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