发明申请
- 专利标题: METHOD AND DEVICE FOR PRODUCING DIMETHYL ETHER FROM METHANOL
- 专利标题(中): 用于从甲醇生产二甲醚的方法和装置
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申请号: US13130611申请日: 2009-11-19
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公开(公告)号: US20110295043A1公开(公告)日: 2011-12-01
- 发明人: Bernd Ahlers , Gerhard Birke , Harald Koempel , Hermann Bach , Martin Rothaemel , Waldemar Liebner , Walter Boll , Veronika Gronemann
- 申请人: Bernd Ahlers , Gerhard Birke , Harald Koempel , Hermann Bach , Martin Rothaemel , Waldemar Liebner , Walter Boll , Veronika Gronemann
- 申请人地址: DE Frankfurt am Main
- 专利权人: LURGI GMBH
- 当前专利权人: LURGI GMBH
- 当前专利权人地址: DE Frankfurt am Main
- 优先权: DE102008058931.4 20081125
- 国际申请: PCT/EP2009/008237 WO 20091119
- 主分类号: C07C41/09
- IPC分类号: C07C41/09 ; B01J19/00
摘要:
A process produces dimethyl ether (DME) from methanol (MeOH). The process includes charging a feed mixture consisting of raw MeOH and a process-internally obtained return flow substantially consisting of unconverted MeOH and reaction water to an MeOH column. The feed mixture is evaporated in the MeOH column to form a first distillate substantially consisting of vaporous MeOH. The first distillate is supplied to a reactor and the MeOH is converted to DME by splitting off water in the reactor so as to form a reaction mixture. The reaction mixture is withdrawn from the reactor, charged to a mixture column and separated into a bottom product substantially consisting of water and a second distillate substantially consisting of DME and MeOH. The second distillate is separated in a DME column into a third distillate substantially consisting of DME, a bottom product consisting essentially of water-poor MeOH, and uncondensable gases discharged overhead. The bottom product is either supplied to a top of the MeOH column or mixed with another bottom product withdrawn from a forerun column.
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