发明申请
- 专利标题: Semi-Continuous Method For Producing Copolymers
- 专利标题(中): 用于生产共聚物的半连续方法
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申请号: US13133026申请日: 2009-11-25
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公开(公告)号: US20120035300A1公开(公告)日: 2012-02-09
- 发明人: Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
- 申请人: Reinhard Dorfner , Klaus Lorenz , Petra Wagner , Christian Scholz
- 优先权: EP08170979.2 20081208
- 国际申请: PCT/EP2009/065790 WO 20091125
- 主分类号: C04B16/04
- IPC分类号: C04B16/04 ; C08F216/14 ; C08F2/10
摘要:
The present invention relates to a process for the preparation of a copolymer in semicontinuous operation in a polymerization apparatus, comprising a polymerization reactor connected to a metering device, in each case acid monomer being initially taken in the metering device and polyether macromonomer and water in the polymerization reactor, acid monomer being metered from the metering device via an acid monomer metering line into the polymerization reactor, free radical polymerization initiator being passed into the polymerization reactor before and/or during the metering of the acid monomer into the polymerization reactor so that an aqueous medium in which acid monomer and polyether macromonomer are reacted with formation of the copolymer by free radical polymerization forms in the polymerization reactor, a portion of the copolymer-containing aqueous medium being passed continuously during the free radical polymerization from the polymerization reactor via a reaction mixture line which is connected via a mixing device to the acid monomer metering line, the discharged copolymer-containing aqueous medium being mixed with the acid monomer in the mixing device during the metering of the acid monomer and being recycled to the polymerization reactor after the mixing via the acid monomer metering line.
公开/授权文献
- US08536285B2 Semi-continuous method for producing copolymers 公开/授权日:2013-09-17
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