发明申请
US20120071620A1 METHOD FOR CRYSTALLIZING (METH)ACRYLIC ACID AND METHOD FOR REGULATING CONTENT OF POLYMERIZATION INHIBITOR IN PRODUCT (METH)ACRYLIC ACID
有权
用于结晶(甲基)丙烯酸的方法和用于调节产物(甲基)丙烯酸中聚合抑制剂含量的方法
- 专利标题: METHOD FOR CRYSTALLIZING (METH)ACRYLIC ACID AND METHOD FOR REGULATING CONTENT OF POLYMERIZATION INHIBITOR IN PRODUCT (METH)ACRYLIC ACID
- 专利标题(中): 用于结晶(甲基)丙烯酸的方法和用于调节产物(甲基)丙烯酸中聚合抑制剂含量的方法
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申请号: US13322633申请日: 2010-05-27
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公开(公告)号: US20120071620A1公开(公告)日: 2012-03-22
- 发明人: Kazuhiko Sakamoto , Koji Ueno , Yoshitake Ishii , Harunori Hirao , Satoshi Nakagawa
- 申请人: Kazuhiko Sakamoto , Koji Ueno , Yoshitake Ishii , Harunori Hirao , Satoshi Nakagawa
- 优先权: JP2009-132000 20090601
- 国际申请: PCT/JP2010/058997 WO 20100527
- 主分类号: C08F120/06
- IPC分类号: C08F120/06 ; C07C51/50
摘要:
PROBLEMThere is provided a melting method of (meth)acrylic acid crystal which is capable of providing a higher quality of (meth)acrylic acid without carrying out an additional purification treatment to (meth)acrylic acid obtained by a crystallization operation accompanied by melting of (meth)acrylic acid. In addition, there is provided a simple method for adjusting a content of polymerization inhibitor in a product (meth)acrylic acid.SOLUTIONIn the crystallization method melting (meth)acrylic acid crystal while wetting with the crystalline molten liquid, a polymerization inhibitor is added to a molten liquid melted after initiation of melting, and all of crystal is melted while circulating and feeding the molten liquid containing said polymerization inhibitor to the crystal. In addition, a content of polymerization inhibitor in product (meth)acrylic acid is adjusted by adding a predetermined amount of polymerization inhibitor corresponding to a product specification to the molten liquid melted after initiation of melting.
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