发明申请
US20120071620A1 METHOD FOR CRYSTALLIZING (METH)ACRYLIC ACID AND METHOD FOR REGULATING CONTENT OF POLYMERIZATION INHIBITOR IN PRODUCT (METH)ACRYLIC ACID 有权
用于结晶(甲基)丙烯酸的方法和用于调节产物(甲基)丙烯酸中聚合抑制剂含量的方法

METHOD FOR CRYSTALLIZING (METH)ACRYLIC ACID AND METHOD FOR REGULATING CONTENT OF POLYMERIZATION INHIBITOR IN PRODUCT (METH)ACRYLIC ACID
摘要:
PROBLEMThere is provided a melting method of (meth)acrylic acid crystal which is capable of providing a higher quality of (meth)acrylic acid without carrying out an additional purification treatment to (meth)acrylic acid obtained by a crystallization operation accompanied by melting of (meth)acrylic acid. In addition, there is provided a simple method for adjusting a content of polymerization inhibitor in a product (meth)acrylic acid.SOLUTIONIn the crystallization method melting (meth)acrylic acid crystal while wetting with the crystalline molten liquid, a polymerization inhibitor is added to a molten liquid melted after initiation of melting, and all of crystal is melted while circulating and feeding the molten liquid containing said polymerization inhibitor to the crystal. In addition, a content of polymerization inhibitor in product (meth)acrylic acid is adjusted by adding a predetermined amount of polymerization inhibitor corresponding to a product specification to the molten liquid melted after initiation of melting.
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