发明申请
US20120296127A1 INTEGRATED PROCESS FOR THE PRODUCTION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE
有权
用于生产1-氯代-3,3,3-三氟乙烯的综合方法
- 专利标题: INTEGRATED PROCESS FOR THE PRODUCTION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE
- 专利标题(中): 用于生产1-氯代-3,3,3-三氟乙烯的综合方法
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申请号: US13471565申请日: 2012-05-15
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公开(公告)号: US20120296127A1公开(公告)日: 2012-11-22
- 发明人: Stephen A. Cottrell , Hsueh Sung Tung , Konstantin A. Pokrovski
- 申请人: Stephen A. Cottrell , Hsueh Sung Tung , Konstantin A. Pokrovski
- 主分类号: C07C21/18
- IPC分类号: C07C21/18 ; C07C17/25
摘要:
The present invention is directed to processes for the production of 1233zd from 240fa and HF, with or without a catalyst, at a commercial scale. The 240fa and HF are fed to a reactor operating at high pressure. The resulting product stream comprising 1233zd, HCl, HF, and other byproducts is treated to one or more purification techniques including phase separation and one or more distillations to provide purified 1233zd, which meets commercial product specifications, i.e., having a GC purity of 99.5% or greater.
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