Invention Application
- Patent Title: Solid-Stage Polymerization System for a Liquid Crystalline Polymer
- Patent Title (中): 液晶聚合物固相聚合体系
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Application No.: US13627374Application Date: 2012-09-26
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Publication No.: US20130085253A1Publication Date: 2013-04-04
- Inventor: Steven D. Gray , Robert Alan Deck , Bing Lu
- Applicant: Ticona LLC
- Applicant Address: US KY Florence
- Assignee: Ticona LLC
- Current Assignee: Ticona LLC
- Current Assignee Address: US KY Florence
- Main IPC: C08G63/80
- IPC: C08G63/80 ; B01J8/18 ; C08G63/06

Abstract:
A multi-stage process for forming a liquid crystalline polymer is provided. More particularly, the process includes acetylating one or more precursor monomers and melt-polymerizing the acetylated monomers to form a prepolymer in the form of a solid particulate material. Thereafter, the prepolymer is solid-state polymerized in a fluidized bed reactor that contains a porous surface (e.g., bed, plate, grate, etc.) on which the prepolymer is supported. While supported by this porous surface, the prepolymer can become “fluidized” with a heated stream of a gas (e.g., nitrogen). In this manner, a sufficient degree of turbulence is created to distribute heat evenly around the prepolymer and cause it to rapidly reach the target reaction temperature.
Public/Granted literature
- US08618239B2 Solid-stage polymerization system for a liquid crystalline polymer Public/Granted day:2013-12-31
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