发明申请
- 专利标题: METHOD FOR PRODUCING EPOXY COMPOUND
- 专利标题(中): 生产环氧化合物的方法
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申请号: US13809786申请日: 2011-06-29
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公开(公告)号: US20130116455A1公开(公告)日: 2013-05-09
- 发明人: Yoshikazu Arai , Hiroshi Uchida
- 申请人: Yoshikazu Arai , Hiroshi Uchida
- 申请人地址: JP Minato-ku, Tokyo
- 专利权人: SHOWA DENKO K.K.
- 当前专利权人: SHOWA DENKO K.K.
- 当前专利权人地址: JP Minato-ku, Tokyo
- 优先权: JP2010-159888 20100714
- 国际申请: PCT/JP2011/064959 WO 20110629
- 主分类号: C07D301/12
- IPC分类号: C07D301/12
摘要:
Provided is a safe and simple method for producing an epoxy compound, wherein a compound with a carbon-carbon double bond is epoxidized by using hydrogen peroxide as an oxidizing agent in the presence of acetonitrile, wherein there is no need for concentration of a reaction mixture that contains residual hydrogen peroxide. A method for producing an epoxy compound wherein a compound with a carbon-carbon double bond is epoxidized by using hydrogen peroxide as an oxidizing agent, in the presence of acetonitrile, comprises a first step of adding water and an organic solvent that is incompatible with water and does not dissolve an acetamide by-product of the epoxidation reaction to a reaction mixture, upon completion of the epoxidation reaction, to dissolve the acetamide in the water, a second step of separating an organic layer and an aqueous layer, and a third step of subjecting the organic layer to reduction treatment, and then rinsing and concentrating it to provide an epoxy compound.
公开/授权文献
- US08759553B2 Method for producing epoxy compound 公开/授权日:2014-06-24
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