发明申请
US20130116455A1 METHOD FOR PRODUCING EPOXY COMPOUND 有权
生产环氧化合物的方法

  • 专利标题: METHOD FOR PRODUCING EPOXY COMPOUND
  • 专利标题(中): 生产环氧化合物的方法
  • 申请号: US13809786
    申请日: 2011-06-29
  • 公开(公告)号: US20130116455A1
    公开(公告)日: 2013-05-09
  • 发明人: Yoshikazu AraiHiroshi Uchida
  • 申请人: Yoshikazu AraiHiroshi Uchida
  • 申请人地址: JP Minato-ku, Tokyo
  • 专利权人: SHOWA DENKO K.K.
  • 当前专利权人: SHOWA DENKO K.K.
  • 当前专利权人地址: JP Minato-ku, Tokyo
  • 优先权: JP2010-159888 20100714
  • 国际申请: PCT/JP2011/064959 WO 20110629
  • 主分类号: C07D301/12
  • IPC分类号: C07D301/12
METHOD FOR PRODUCING EPOXY COMPOUND
摘要:
Provided is a safe and simple method for producing an epoxy compound, wherein a compound with a carbon-carbon double bond is epoxidized by using hydrogen peroxide as an oxidizing agent in the presence of acetonitrile, wherein there is no need for concentration of a reaction mixture that contains residual hydrogen peroxide. A method for producing an epoxy compound wherein a compound with a carbon-carbon double bond is epoxidized by using hydrogen peroxide as an oxidizing agent, in the presence of acetonitrile, comprises a first step of adding water and an organic solvent that is incompatible with water and does not dissolve an acetamide by-product of the epoxidation reaction to a reaction mixture, upon completion of the epoxidation reaction, to dissolve the acetamide in the water, a second step of separating an organic layer and an aqueous layer, and a third step of subjecting the organic layer to reduction treatment, and then rinsing and concentrating it to provide an epoxy compound.
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