发明申请
- 专利标题: METHOD FOR PRODUCING POLYLACTIC ACID
- 专利标题(中): 生产聚酸的方法
-
申请号: US13704793申请日: 2011-06-16
-
公开(公告)号: US20130178598A1公开(公告)日: 2013-07-11
- 发明人: Hisanori Kishida , Takashi Hasegawa , Kenji Miyaguchi , Takehiko Moriya , Nobuyoshi Nomura , Ryohei Ogawa
- 申请人: Hisanori Kishida , Takashi Hasegawa , Kenji Miyaguchi , Takehiko Moriya , Nobuyoshi Nomura , Ryohei Ogawa
- 申请人地址: JP Osaka-shi JP Nagoya-shi JP Sendai-shi
- 专利权人: HITACHI ZOSEN CORPORATION,NATIONAL UNIVERSITY CORPORATION NAGOYA UNIVERSITY,TOHOKU ELECTRIC POWER CO., INC.
- 当前专利权人: HITACHI ZOSEN CORPORATION,NATIONAL UNIVERSITY CORPORATION NAGOYA UNIVERSITY,TOHOKU ELECTRIC POWER CO., INC.
- 当前专利权人地址: JP Osaka-shi JP Nagoya-shi JP Sendai-shi
- 优先权: JP2010-137992 20100617
- 国际申请: PCT/JP2011/063811 WO 20110616
- 主分类号: C08G63/84
- IPC分类号: C08G63/84
摘要:
To provide a method capable of producing stereocomplex polylactic acid, the method being capable of using carbon neutral materials that are not competitive from foods, such as saccharides, without the use of a method for designing optical resolution, which requires complicated operations and high cost and is difficult to perform mass production. The production method of the present invention comprises: a step of reacting glycerin with sodium hydroxide in high-temperature and high-pressure water to produce a racemic sodium lactate aqueous solution; a step of separating sodium from the racemic sodium lactate aqueous solution to recover racemic lactic acid; a step of dimerizing the racemic lactic acid to produce a lactide mixture containing meso lactide and racemic lactide; a step of separating meso lactide from the mixture to recover racemic lactide; and a step of polymerizing the racemic lactide with a salen-metal complex as a catalyst to produce stereocomplex polylactic acid.
公开/授权文献
- US09056946B2 Method for producing polylactic acid 公开/授权日:2015-06-16
信息查询