发明申请
- 专利标题: NOBLE METAL SUPERPARTICLES AND METHODS OF PREPARATION THEREOF
- 专利标题(中): NOBLE金属超级制剂及其制备方法
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申请号: US14600908申请日: 2015-01-20
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公开(公告)号: US20160208360A1公开(公告)日: 2016-07-21
- 发明人: Yugang Sun , Yongxing Hu
- 申请人: UChicago Argonne, LLC
- 申请人地址: US IL Chicago
- 专利权人: UChicago Argonne, LLC
- 当前专利权人: UChicago Argonne, LLC
- 当前专利权人地址: US IL Chicago
- 主分类号: C22B3/00
- IPC分类号: C22B3/00 ; B01J23/38 ; B01J23/42 ; C22C5/04 ; B01J23/46 ; B01J35/00 ; B22F9/24 ; B01J35/02 ; B01J23/44
摘要:
A method comprises heating an aqueous solution of colloidal silver particles. A soluble noble metal halide salt is added to the aqueous solution which undergoes a redox reaction on a surface of the silver particles to form noble metal/silver halide SPs, noble metal halide/silver halide SPs or noble metal oxide/silver halide SPs on the surface of the silver particles. The heat is maintained for a predetermined time to consume the silver particles and release the noble metal/silver halide SPs, the noble metal halide/silver halide SPs or the noble metal oxide/silver halide SPs into the aqueous solution. The aqueous solution is cooled. The noble metal/silver halide SPs, the noble metal halide/silver halide SPs or noble metal oxide/silver halide SPs are separated from the aqueous solution. The method optionally includes adding a soluble halide salt to the aqueous solution.
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