• Patent Title: SOLIDIFICATION OF HEXYL 2-[4-(DIETHYLAMINO)-2-HYDROXYBENZOYL]BENZOATE
  • Application No.: US18279899
    Application Date: 2022-03-01
  • Publication No.: US20240150276A1
    Publication Date: 2024-05-09
  • Inventor: Daniel Ruben SELZEREva KLEINMANNAxel BINDERHelmut KRONEMAYERPhilipp STAEHLE
  • Applicant: BASF SE
  • Applicant Address: DE Ludwigshafen am Rhein
  • Assignee: BASF SE
  • Current Assignee: BASF SE
  • Current Assignee Address: DE Ludwigshafen am Rhein
  • Priority: EP 160497.0 2021.03.03
  • International Application: PCT/EP2022/055089 2022.03.01
  • Date entered country: 2023-09-01
  • Main IPC: C07C229/52
  • IPC: C07C229/52
SOLIDIFICATION OF HEXYL 2-[4-(DIETHYLAMINO)-2-HYDROXYBENZOYL]BENZOATE
Abstract:
The present invention relates to a process for the solidification of hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate (INCI diethylamino hydroxybenzoyl hexyl benzoate, DHHB), wherein the process comprises the step of (a) applying a shear rate of 800 s−1 or more to liquid hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate and (b) adding seed crystals of hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate.
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