发明授权
- 专利标题: N-substituted .epsilon.-caprolactams
- 专利标题(中): N-取代的ε-己内酰胺
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申请号: US967593申请日: 1978-12-08
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公开(公告)号: US4185017A公开(公告)日: 1980-01-22
- 发明人: Steffen Piesch , Herbert Wille
- 申请人: Steffen Piesch , Herbert Wille
- 申请人地址: DEX Frankfurt
- 专利权人: Cassella Aktiengesellschaft
- 当前专利权人: Cassella Aktiengesellschaft
- 当前专利权人地址: DEX Frankfurt
- 优先权: DEX2755588 19771214
- 主分类号: C07D223/10
- IPC分类号: C07D223/10 ; C08G12/04 ; C08G12/40 ; D21H17/49
摘要:
Condensation products of .epsilon.-caprolactam, formaldehyde and formamide, especially N-(formylaminomethyl)-.epsilon.-caprolactam and N-(N'-formyl-N'-hydroxymethyl-aminomethyl)-.epsilon.-caprolactam, are prepared by reacting formamide and formaldehyde in the presence of a base and in the presence or absence of .epsilon.-caprolactam at temperatures of 70.degree. to 90.degree. C. for 4 to 15 hours, then acidifying the reaction batch and, if no .epsilon.-caprolactam is present, adding .epsilon.-caprolactam, and distilling off water at 100.degree. to 135.degree. C.The condensation products are valuable modifiers for use in the manufacture of aminoplast resins employed for impregnating paper and fabrics which are used for the manufacture of coated wood-based materials and laminates.
公开/授权文献
- US5309469A Monitoring optical gain of semiconductor optical amplifier 公开/授权日:1994-05-03
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