发明授权
- 专利标题: Preparation of anilino azo carbazole dyestuffs prepared by diazotization by nitrosylsulphuric acid in acetic acid
- 专利标题(中): 通过硝酸基硫酸在乙酸中重氮化制备的苯胺基偶氮咔唑染料
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申请号: US410138申请日: 1982-08-20
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公开(公告)号: US4472307A公开(公告)日: 1984-09-18
- 发明人: Ulrich Buhler , Wolfgang Bodenstedt , Heinz Hanel , Eberhardt Hebestreit , Horst Tappe
- 申请人: Ulrich Buhler , Wolfgang Bodenstedt , Heinz Hanel , Eberhardt Hebestreit , Horst Tappe
- 申请人地址: DEX Frankfurt am Main
- 专利权人: Cassella Aktiengesellschaft
- 当前专利权人: Cassella Aktiengesellschaft
- 当前专利权人地址: DEX Frankfurt am Main
- 优先权: DEX3140716 19811014
- 主分类号: C09B29/40
- IPC分类号: C09B29/40 ; C09B41/00 ; C09B29/01
摘要:
An improved process for the preparation of azo dyestuffs of the formula ##STR1## comprising diazotizing a 2-halo-4-nitroaniline at 10.degree. to 35.degree. C. in 70 to 100 percent by weight strength acetic acid by means of nitrosylsulphuric acid, adjusting the acetic acid content of the resulting diazo solution to 60 to 85% by the addition of water, and at a temperature from 15.degree. to 45.degree. C. adding an appropriate carbazole to the diazo solution as a solid or in the form of a suspension in 60 to 100 percent strength by weight acetic acid and coupling the carbazole to the diazotized amine to produce said azo dyestuff and isolating the dyestuff.
公开/授权文献
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