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US4499277A Reduction of trichloromethylpyridines to dichloromethylpyridines 失效
将三氯甲基吡啶还原成二氯甲基吡啶

Reduction of trichloromethylpyridines to dichloromethylpyridines
摘要:
2(6)-(Trichloromethyl)pyridines are reduced to the corresponding 2(6)-(dichloromethyl)pyridines by treatment with a strong base and an anionic reductant derived from a reductant source material selected from the group consisting of dialkylphosphite and trialkylphosphite said treatment taking place in the presence of a polar, non-hydroxylic solvent and/or a phase transfer catalyst.
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