发明授权
- 专利标题： Method for producing chlorosulfonated polyethylene with controlling addition amount of sulfur of the chlorosulfonated polyethylene
- 专利标题（中）： 控制氯磺化聚乙烯硫添加量的氯磺化聚乙烯生产方法
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申请号： US702434申请日： 1985-02-19
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公开(公告)号： US4663396A公开(公告)日： 1987-05-05
- 发明人: Tatsushi Nakagawa , Mamoru Narui , Yasuhiro Sakanaka
- 申请人： Tatsushi Nakagawa , Mamoru Narui , Yasuhiro Sakanaka
- 申请人地址： JPX Yamaguchi
- 专利权人： Toyo Soda Manufacturing Co., Ltd.
- 当前专利权人： Toyo Soda Manufacturing Co., Ltd.
- 当前专利权人地址： JPX Yamaguchi
- 优先权： JPX57-142075 19820818
- 主分类号： C08F8/00
- IPC分类号： C08F8/00 ; C08F8/38
摘要：
A method for producing chlorosulfonated polyethylene with controlled addition of the amount of sulfur added to the polyethylene. Polyethylene dissolved in halogenated hydrocarbon is reacted with sulfuryl chloride in the presence of a catalyst of a radical generating agent in a binary phase system. The addition amount of sulfur is controlled by adding an amine compound to the reaction in an amount within the range where the following formula is applicable:log.sub.10 S=.alpha..multidot.log.sub.10 A+.beta. (1)whereinS: reaction yield (%) of sulfur of sulfuryl chlorideA: concentration (mol/liter) of amine compound in halogenated hydrocarbon solvent.alpha.,.beta.: constants such that1.0
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