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US4748126A Pyridine-free Karl-Fischer reagent and a process for the determination of water therewith 失效
不含吡啶的卡尔费休试剂及其测定方法

Pyridine-free Karl-Fischer reagent and a process for the determination
of water therewith
摘要:
A pyridine-free Karl-Fischer reagent for the determination of water which comprises (a) a solvent solution containing sulfur dioxide and an amine in a Karl-Fischer reagent solvent, the amine being functionally equivalent to pyridine in a Karl-Fischer reagent, and (b) a titrating agent containing iodine in a Karl-Fischer solvent; the molar ratio of amine to sulfur dioxide being about 2:1 to about 1:1 and the reagent being essentially free of pyridine.
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