发明授权
- 专利标题: Method of making translucent alumina articles
- 专利标题(中): 制作半透明氧化铝制品的方法
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申请号: US255564申请日: 1988-10-11
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公开(公告)号: US4948538A公开(公告)日: 1990-08-14
- 发明人: George C. Wei , William H. Rhodes
- 申请人: George C. Wei , William H. Rhodes
- 申请人地址: MA Waltham
- 专利权人: GTE Laboratories Incorporated
- 当前专利权人: GTE Laboratories Incorporated
- 当前专利权人地址: MA Waltham
- 主分类号: C04B35/115
- IPC分类号: C04B35/115 ; C04B35/64
摘要:
A method of making a translucent alumina article is described. The method comprises the following steps:Step 1 - An alumina powder and a sintering aid are mixed in a liquid for a period sufficient to form a homogeneous slurry.Step 2 - The homogeneous slurry from Step 1 is dried remove the liquid to form a dried powder.Step 3 - The dried powder is shaped to form a compacted green body.Step 4 - The compacted green body from Step 3 is heated at a temperature equal to or less than 500.degree. C. and for a period sufficient to form a compacted green body having a density of at least 30% of theoretical density.Step 5 - The compacted green body having a density of at least 30% of theoretical density from Step 4 is heated at a temperature from about 800.degree. C. to about 1300.degree. C. in an oxygen containing atmosphere for a period sufficient to impart green strength to said compacted green body to form a prefired compacted green body.Step 6 - The prefired compacted green body from Step 5 is sintered at a temperature from about 1700.degree. C., to about 2000.degree. C. in an nitrogen/hydrogen atmosphere consisting essentially of nitrogen and hydrogen for a period sufficient to form a translucent polycrystalline alumina article, the hydrogen being equal to or greater than about one volume percent of said nitrogen/hydrogen atmosphere and having a dew point in the range of minus 15.degree. C. to about minus 110.degree. C.
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