发明授权
- 专利标题: Synthesis of aminonitrobenzodifuroxan
- 专利标题(中): 氨基硝基苯并二呋喃的合成
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申请号: US593413申请日: 1990-10-01
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公开(公告)号: US5149818A公开(公告)日: 1992-09-22
- 发明人: Stephen L. Christian , Andrew P. Chafin , Arnold T. Nielsen , Ronald L. Atkins , William P. Norris , Richard A. Hollins
- 申请人: Stephen L. Christian , Andrew P. Chafin , Arnold T. Nielsen , Ronald L. Atkins , William P. Norris , Richard A. Hollins
- 申请人地址: DC Washington
- 专利权人: The United States of America as represented by the Secretary of the Navy
- 当前专利权人: The United States of America as represented by the Secretary of the Navy
- 当前专利权人地址: DC Washington
- 主分类号: C07D498/04
- IPC分类号: C07D498/04
摘要:
Aminonitrobenzodifuroxan (CL-18) is prepared by directly converting pentanitroaniline to aminonitrobenzodifuroxan with heat in the presence of an excess of sodium azide. The pentanitroaniline is prepared in high yield from 3,5-dinitroaniline with a mixture of nitric acid and sulfuric acid in which the final sulfuric acid concentration is from 99.0 to 99.5%.
公开/授权文献
- US5762343A Slide ring seal assembly 公开/授权日:1998-06-09
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